Characterization of inclusions in KD2PO4 crystals

被引:10
|
作者
Chang, Junxiu [1 ,2 ]
Zhao, Yuan [1 ]
Hu, Guohang [1 ]
Wang, Yueliang [1 ,2 ]
Li, Dawei [1 ]
Liu, Xiaofeng [1 ]
Shao, Jianda [1 ]
机构
[1] Chinese Acad Sci, Shanghai Inst Opt & Fine Mech, Key Lab Mat High Power Laser, Shanghai 201800, Peoples R China
[2] Univ Chinese Acad Sci, Beijing 100039, Peoples R China
基金
中国国家自然科学基金;
关键词
LASER-INDUCED DAMAGE; RAPID GROWTH; LIQUID INCLUSIONS; KDP; KH2PO4; SUPERSATURATION; SCATTER; ADP;
D O I
10.3788/COL201513.081601
中图分类号
O43 [光学];
学科分类号
070207 ; 0803 ;
摘要
The inclusions in conventionally grown KD2PO4 (DKDP) crystals are investigated. The inclusions are captured by a light-scattering technique. The sizes are determined by an optical microscope and a transmission electron microscope (TEM), and the compositions are analyzed by time of flight secondary ion mass spectrometry (TOF-SIMS) and an energy dispersive spectrometer (EDS). Two kinds of inclusions are observed in the DKDP crystals: a submicron-scale inclusion and a micron-scale inclusion. The typical submicron-scale inclusions contain growth solution, and their sizes range from tens to hundreds of nanometers, whereas the micron-scale inclusions contain growth solution and the metal element Na, and the sizes are tens of microns. The possible formation mechanisms of the inclusions are discussed, and the influence of the inclusions on laser-induced damage behaviors are analyzed and discussed.
引用
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页数:4
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