N,N-Bis(quinolin-8-yl)-2,2′-[(1,3,4-thiadiazole-2,5-diyl)bis(sulfanediyl)]diacetamide monohydrate

被引：1
|
作者：
Li, Xiao-Feng [2 ]
An, Yan [2 ]
Huang, Qing-Hua [1 ]
Wen, Yong-Hong [1 ]
机构：
[1] Qingdao Univ Sci & Technol, Coll Chem & Mol Engn, Qingdao 266042, Peoples R China
[2] Shanghai Maritime Univ, Inst Marine Mat Sci & Engn, Shanghai 201305, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2011年 / 67卷
关键词：
data-to-parameter ratio = 13.6; mean σ(C-C) = 0.003 Å; R factor = 0.044; single-crystal X-ray study; T = 293 K; wR factor = 0.109;
D O I：
10.1107/S1600536811047222
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C24H18N6O2S3 center dot H2O, the thiadiazole ring makes dihedral angles of 78.00 (13) and 77.27 (13)degrees with the quinoline ring systems. In the crystal, molecules are linked into a two-dimensional network by O-H center dot center dot center dot O and C-H center dot center dot center dot O hydrogen bonds.
引用
收藏
页码：O3291 / U510
页数：12
相关论文
共 50 条
  • [1] 2,2 '-[(1,3,4-Thiadiazole-2,5-diyl)bis-(sulfanediyl)]diacetonitrile
    Mague, Joel T.
    Akkurt, Mehmet
    Mohamed, Shaaban K.
    El-Saghier, Ahmed M. M.
    Albayati, Mustafa R.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O1855 - +
  • [2] N,N′-Dibenzyl-2,2′-[(1,3,4-oxadiazole-2,5-diyl)bis(o-phenyleneoxy)]diacetamide
    Wang, Wei
    Huang, Yong
    Tang, Ning
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O2237 - U3061
  • [3] 4,4′-[(1,3,4-thiadiazole-2,5-diyl)bis(thiomethylene)]dibenzonitrile
    Wang, Wenxiang
    Zhao, Hong
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1599 - U3208
  • [4] Synthesis and structure of dihydrazones obtained from the dihydrazide of S,S′-(1,3,4-thiadiazole-2,5-diyl)bis(2-mercaptopropionic acid)
    Rutavichyus A.
    Valyulene S.
    Chemistry of Heterocyclic Compounds, 1998, 34 (12) : 1436 - 1441
  • [5] STRUCTURE OF MONONUCLEAR BIS(AQUA[2,2'-(1,3,4-OXADIAZOLE-2,5-DIYL)DIPYRIDINE-N,N'])COPPER(II) DIPERCHLORATE
    WIGNACOURT, JP
    SUEUR, S
    LAGRENEE, M
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 1990, 46 : 394 - 396
  • [6] New diformazans obtained on the basis of S,S′-(1,3,4-thiadiazole-2,5-diyl)bis(mercaptoacetic) or (2-mercaptopropionic)acid dihydrazides
    Rutavichyus, A
    Valyulene, S
    KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII, 2000, (04): : 547 - 550
  • [7] Synthesis and properties of dihydrazones obtained on the basis of S,S′-(1,3,4-thiadiazole-2,5-diyl)bis(2-mercaptopropionic acid) dihydrazide
    Rutavichius, A
    Valiulene, S
    KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII, 1998, (12): : 1690 - 1695
  • [8] Crystal structure of (3E,3′E)-3,3′-((1,3,4-thiadiazole-2,5-diyl)bis(sulfanediyl))bis(4-hydroxy-4-phenylbut-3-en-2-one), C22H18N2O4S3
    Zeng, Jieqiong
    Zuo, Zhenyu
    Huang, Weiping
    Huang, Shaojun
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2020, 235 (03): : 645 - 646
  • [9] Bis[4-nitro-N-(quinolin-8-yl)benzenesulfonamidato-κ2 N,N′]copper(II)
    da Silva, LE
    Joussef, AC
    Foro, S
    Schmidt, B
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : M518 - M519
  • [10] COMPLEXES OF RHODIUM (3) AND PALLADIUM (2) WITH 1,3,4-THIADIAZOLE-2,5-BIS-T-OCTYLDISULPHIDE
    PNEVMATICAKIS, GA
    STATHIS, EC
    FIELDS, EK
    JOURNAL OF INORGANIC & NUCLEAR CHEMISTRY, 1965, 27 (04): : 895 - +
12345