Modulated temperature DSC measurements: The influence of the experimental conditions

被引：79
|
作者：
Schawe, JEK
机构：
[1] Universität Ulm, Sektion für Kalorimetrie
来源：
THERMOCHIMICA ACTA | 1996年 / 271卷
关键词：
modulated temperature DSC; glass transition; cold crystallization; melting; experimental conditions;
D O I：
10.1016/0040-6031(95)02562-6
中图分类号：
O414.1 [热力学];
学科分类号：
摘要：
The influence of the experimental conditions on the results by modulated temperature DSC (MT-DSC) are investigated. The factors considered are temperature amplitude, frequency, underlying heating rates and sample preparation. Based on theoretical considerations and experimental results, practical recommendations are developed.
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页码：127 / 140
页数：14
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