Ceramization of Carborane-POSS and Coating on Carbon Fiber via Precursor Infiltration-Pyrolysis (PIP) Method

被引：4
|
作者：
Sun, Yi [1 ]
Tong, Dejin [1 ]
Li, Zhanxiong [1 ,2 ]
机构：
[1] Soochow Univ, Coll Text & Clothing Engn, Suzhou 215021, Peoples R China
[2] Natl Engn Lab Modern Silk, Suzhou 215123, Peoples R China
来源：
FIBERS AND POLYMERS | 2019年 / 20卷 / 08期
基金：
中国国家自然科学基金;
关键词：
Carbon fibers; Coating; PIP; Micro-structure; Oxidation resistance; OXIDATION; ZIRCONIUM; CARBIDE; GEL; STABILITY; HAFNIUM; MATRIX;
D O I：
10.1007/s12221-019-8898-8
中图分类号：
TB3 [工程材料学]; TS1 [纺织工业、染整工业];
学科分类号：
0805 ; 080502 ; 0821 ;
摘要：
A novel carborane-POSS pre-polymer has been synthesized and characterized as precursor for ceramic and applied on the surface treatment of carbon fiber by precursor infiltration and pyrolysis (PIP) method. The ceramization transformation process was investigated by using TGA, DSC, Py-GC/MS, etc. Ceramic yield after heating up to 1000 degrees C in nitrogen was 74.3 % and the produced ceramics exhibit excellent thermal and thermo-oxidative stability. Mechanical measurement revealed that the coated carbon fiber maintained 81.22 % of its original tensile strength, and was stable under high temperature in flowing air up to 600 degrees C.
引用
收藏
页码：1564 / 1576
页数：13
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