Synthesis of 13C-labelled, bicyclic mimetics of natural enediynes

被引：10
|
作者：
Das, P
Mita, T
Lear, MJ
Hirama, M [1 ]
机构：
[1] Tohoku Univ, Grad Sch Sci, Dept Chem, Sendai, Miyagi 9808578, Japan
[2] Japan Sci & Technol Corp, CREST, Sendai, Miyagi 9808578, Japan
来源：
CHEMICAL COMMUNICATIONS | 2002年 / 22期
关键词：
D O I：
10.1039/b208939d
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Using a versatile synthesis with (CH3PPh3I)-C-13 and (CH3CO2Et)-C-13 as C-13 sources, the first examples of nine-membered chromophores which have been differentially labelled with C-13 in their carbocyclic enediyne cores are described.
引用
收藏
页码：2624 / 2625
页数：2
相关论文
共 50 条
  • [1] Synthesis of 13C-labelled tetramethyltetraselenafulvalene
    Christensen, JB
    Bechgaard, K
    Paquignon, G
    [J]. JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS, 2001, 44 (14): : 1035 - 1041
  • [2] Synthesis of 13C-labelled cinnamonitrile
    Zippi, EM
    Kamperman, E
    [J]. JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS, 2002, 45 (02): : 103 - 106
  • [3] Synthesis of selectively 13C-labelled bilin compounds
    Makhynya, Yevgen
    Hussain, Zakir
    Bauschlicher, Tanja
    Schwinte, Pascale
    Siebert, Friedrich
    Gaertner, Wolfgang
    [J]. EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2007, 2007 (08) : 1287 - 1293
  • [4] STUDIES TOWARDS THE SYNTHESIS OF 13C-LABELLED ANTHOCYANINS
    Marshall, Laura J.
    Cable, Karl M.
    Botting, Nigel P.
    [J]. JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS, 2010, 53 (5-6): : 315 - 318
  • [5] Synthesis of 11C/13C-labelled prostacyclins
    Bjorkman, M
    Andersson, Y
    Doi, H
    Kato, K
    Suzuki, M
    Noyori, R
    Watanabe, Y
    Langstrom, B
    [J]. ACTA CHEMICA SCANDINAVICA, 1998, 52 (05): : 635 - 640
  • [6] STUDIES TOWARDS THE SYNTHESIS OF 13C-LABELLED ANTHOCYANINS
    Marshall, Laura J.
    Cable, Karl M.
    Botting, Nigel P.
    [J]. JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS, 2010, 53 (7-8): : 523 - 524
  • [7] Synthesis of 11C/13C-labelled prostacyclins
    [J]. Acta Chem Scand, 5 (635-640):
  • [8] Synthesis of [phenyl-13C6]lachnanthocarpone and other 13C-labelled phenylphenalenones
    Otálvaro, F
    Quiñones, W
    Echeverri, F
    Schneider, B
    [J]. JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS, 2004, 47 (02): : 147 - 159
  • [9] Synthesis of doubly 13C-labelled antalarmin isotopomers for pharmacokinetic studies
    Greiner, E
    Atkinson, AJ
    Ayala, A
    Chrousos, GP
    Contoreggi, C
    Eckelman, WC
    Gold, PW
    Habib, KE
    Jacobson, AE
    Whittaker, N
    Webster, EL
    Rice, KC
    [J]. JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS, 2002, 45 (08): : 637 - 645
  • [10] Total synthesis of isotopically labelled flavonoids, 2 -: 13C-labelled (±)-catechin from potassium [13C]cyanide
    Nay, B
    Amaudinaud, V
    Peyrat, JF
    Nuhrich, A
    Deffieux, G
    Mérillon, JM
    Vercauteren, J
    [J]. EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2000, 2000 (07) : 1279 - 1283
12345