Determination of β -sitosterol with Chemical Course and Material Applications in Jatropha Seed Oil by High Performance Liquid Chromatography

被引：4
|
作者：
Liu, ShuYu [1 ]
Maihemuti, ANaErGuLi [1 ]
机构：
[1] Shanghai Univ Engn Sci, Shanghai 201620, Peoples R China
来源：
ENERGY MATERIAL, CHEMICAL ENGINEERING AND MINING ENGINEERING | 2012年 / 577卷
关键词：
Jatropha; sitosterol; Chromatography;
D O I：
10.4028/www.scientific.net/AMR.577.69
中图分类号：
TE [石油、天然气工业]; TK [能源与动力工程];
学科分类号：
0807 ; 0820 ;
摘要：
A simple and rapid high performance liquid chromatography (HPLC) assay was developed to identify and measure the beta -sitosterol with chemical course and material applications in jatropha seed oil. The stigmasterol was isolated with a good selectivity by HPLC employing reversed phase C18 columns. The components were separated by mobile phase of methanol-water (99/1, v/v) and detected at 205mn. The quantitation of the stigmasterol was reproducible and the method relative standard deviation is 1.1%. The mean analytical recovery was 96.2%.
引用
收藏
页码：69 / 72
页数：4
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