Ultra-trace-level determination of the antifouling agent Irgarol 1051 by gas chromatography with tandem mass spectrometric detection

被引：41

作者：

Steen, RJCA ^{[1
]}

Leonards, PEG ^{[1
]}

Brinkman, UAT ^{[1
]}

Cofino, WP ^{[1
]}

机构：

[1] VRIJE UNIV AMSTERDAM,DEPT ANALYT CHEM,NL-1081 HV AMSTERDAM,NETHERLANDS

来源：

JOURNAL OF CHROMATOGRAPHY A | 1997年 / 766卷 / 1-2期

关键词：

programmed-temperature vaporizer; environmental analysis; water analysis; Irgarol; 1051; pesticides; triazines;

D O I：

10.1016/S0021-9673(96)01039-4

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

The contamination level of the s-triazine herbicide Irgarol 1051, which is used as the active ingredient in antifouling paints, was studied in the Western Scheldt estuary. The combined use of large-volume injection gas chromatography and ion trap (MS-MS) detection, enabled identification and quantification at the 0.1-1 ng/l level. By using tandem mass spectrometric detection (MS-MS), rather than conventional MS, a great gain in selectivity was achieved. The concentration levels found ranged between 1 and 10 ng/l.

引用

页码：153 / 158

页数：6

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