Three-component reaction between trivalent phosphorus nucleophiles, dialkyl acetylenedicarboxylates and (2,4-dinitrophenyl) acetic acid

被引：2
|
作者：
Hassanabadi, Alireza [1 ]
Mosslemin, Mohammad H. [2 ]
Abyar, Elaheh [2 ]
Taleb-Malamiri, Mohammad [2 ]
机构：
[1] Islamic Azad Univ, Dept Chem, Zahedan Branch, Zahedan, Iran
[2] Islamic Azad Univ, Dept Chem, Yazd Branch, Yazd, Iran
来源：
JOURNAL OF CHEMICAL RESEARCH | 2012年 / 08期
关键词：
(2,4-dinitrophenyl)acetic acid; dialkyl acetylenedicarboxylate; phosphites; stereoselective synthesis; phosphorus ylides; triphenylphosphine; ONE-POT SYNTHESIS; DIMETHYL ACETYLENEDICARBOXYLATE; PHOSPHITES; DERIVATIVES;
D O I：
10.3184/174751912X13403013285904
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A three-component reaction between dialkyl acetylenedicarboxylates (DAADs) and phosphites in the presence of (2,4-dinitrophenyl) acetic acid leads to dialkyl 2-(dialkoxyphosphoryl)-3-[3-acetyl-2-(2,4-dinitrophenyl)-4-oxosuccinates in excellent yields. A similar reaction with triphenylphosphine, instead of phosphites, produces the stabilised phosphoranes in good yields.
引用
收藏
页码：497 / 499
页数：3
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