A FACILE SYNTHESIS OF 3-(1H-BENZIMIDAZOL-2-YL)-CHROMEN-2-ONES

被引:0
|
作者
Babu, P. N. Kishore [1 ]
Tasqeeruddin, S. [1 ]
Ramadevi, B. [1 ]
Dubey, P. K. [1 ]
机构
[1] Jawaharlal Nehru Technol Univ, Dept Chem, Coll Engn, Hyderabad 500085, Andhra Pradesh, India
关键词
DERIVATIVES; COUMARINS; AGENTS;
D O I
暂无
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
A facile synthesis of 3-(1H-benzimidazol-2-yl)-chromen-2-ones (3) by the reaction of salicylaldehyde (1) with ethyl (1H-benzimidazol-2-yl)-acetate (2) is being reported. The reactions have been done under conventional, solid phase (i.e. physical grinding) as well as under microwave conditions. The latter procedure has been found to be much more efficient in terms of yield and time. The structure of all the products have been established by their spectral and analytical data.
引用
收藏
页码:289 / 292
页数:4
相关论文
共 50 条
  • [1] A Facile and Efficient Synthesis of 3-(1H-Benzimidazol-2-yl)chromen-2-ones
    Tasqeeruddin, S.
    Dubey, P. K.
    [J]. ASIAN JOURNAL OF CHEMISTRY, 2011, 23 (07) : 3297 - 3298
  • [2] MICROWAVE ASSISTED SYNTHESIS OF 3-[2-(1H-BENZIMIDAZOL-2-YL-SULFANYL)-ACETYL]-CHROMEN-2-ONES
    Dubey, P. K.
    Kumar, N. D. Mahesh
    Chaitanya, M. V. S. R. K.
    Tasqeeruddin, Syed
    [J]. INDIAN JOURNAL OF HETEROCYCLIC CHEMISTRY, 2010, 19 (03) : 285 - 286
  • [3] ONE-POT SYNTHESIS AND METHYLATION OF 3-[2-(1H-BENZIMIDAZOL-2-YL-SULFANYL)-ACETYL]-CHROMEN-2-ONES
    Tasqeeruddin, S.
    Dubey, P. K.
    [J]. PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2012, 187 (01) : 128 - 134
  • [4] IODINE CATALYZED ONE POT SYNTHESIS OF 3-[2-(1H-BENZIMIDAZOL-2-YL-SULFANYL)-ACETYL]-CHROMEN-2-ONES
    Srikrishna, D.
    Tasqeeruddin, S.
    Dubey, P. K.
    [J]. INDIAN JOURNAL OF HETEROCYCLIC CHEMISTRY, 2012, 21 (03) : 245 - 250
  • [5] 3-[(1H-Benzimidazol-2-yl)sulfanylmethyl]benzonitrile
    Lin, Jin Rui
    He, Jia
    Qian, Yang
    Zhao, Hong
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O1358 - U2563
  • [6] Bis[μ-3-(1H-benzimidazol-2-yl)benzoato]dicopper(I)
    Lei, Ke-Wei
    Xia, Dong-Guo
    Li, Jie
    Su, Zheng-Yu
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : M1582 - U930
  • [7] Synthesis and photoinduced fluorescence of 3-(2-hetarylethenyl)chromen-2-ones
    A. Yu. Bochkov
    V. N. Yarovenko
    M. M. Krayushkin
    T. A. Chibisova
    T. M. Valova
    V. A. Barachevskii
    V. F. Traven’
    I. P. Beletskaya
    [J]. Russian Journal of Organic Chemistry, 2008, 44 : 595 - 601
  • [8] Synthesis and photoinduced fluorescence of 3-(2-hetarylethenyl)chromen-2-ones
    Bochkov, A. Yu.
    Yarovenko, V. N.
    Krayushkin, M. M.
    Chibisova, T. A.
    Valova, T. M.
    Barachevskii, V. A.
    Traven, V. F.
    Beletskaya, I. P.
    [J]. RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2008, 44 (04) : 595 - 601
  • [9] 3-(1H-Benzimidazol-2-yl)-2-chloro-8-methylquinoline
    Rominger, Frank
    Malathi, Mahalingam
    Mohan, Palathurai Subramaniam
    Dondeti, Tanuja Ramamurthi
    Hashmi, A. Stephen K.
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O400 - U2848
  • [10] SYNTHESIS OF NEW 3-(1-ARYL-2-THIOXO-3,4-DIHYDRO-2H-IMIDAZOL-4-YL) CHROMEN-2-ONES
    Soman, Shubhangi S.
    Thaker, Tirth H.
    [J]. INDIAN JOURNAL OF HETEROCYCLIC CHEMISTRY, 2009, 19 (01) : 55 - 58