X-ray crystal structure of disazo dyes .2. Derivatives of CI Disperse Yellow 23 and CI Disperse Orange 29

被引:12
|
作者
Freeman, HS [1 ]
McIntosh, SA [1 ]
Singh, P [1 ]
机构
[1] N CAROLINA STATE UNIV,DEPT CHEM,RALEIGH,NC 27695
关键词
crystal structure; diazo dyes; anti-conformation; monoclinic;
D O I
10.1016/S0143-7208(96)00096-4
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
Crystals of the 2,6-dichlorobenzoyl ester of C.I. Disperse Yellow 23 and C.I. Disperse Orange 29 were grown from chloroform, and cell dimensions were determined by a least-squares fit. Crystals of both esters were found to exist in the monoclinic space group P2(1)/C. The structures of these dyes possessed the anti conformation, unlike that of underivatized C.I. Disperse Orange 29, but the same as that reported for 4-phenylazoazobenzene. (C) 1997 Elsevier Science Ltd.
引用
收藏
页码:149 / 164
页数:16
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