Silver, gold and the corresponding core shell nanoparticles: synthesis and characterization

被引：37
|
作者：
Douglas, Fraser [2 ]
Yanez, Ramon [2 ]
Ros, Josep [2 ]
Marin, Sergio [1 ,3 ]
de la Escosura-Muniz, Alfredo [3 ]
Alegret, Salvador [1 ]
Merkoci, Arben [1 ,3 ]
机构：
[1] Univ Autonoma Barcelona, Grp Sensors & Biosensors, Dept Quim, Bellaterra 08193, Catalonia, Spain
[2] Univ Autonoma Barcelona, Unitat Quim Inorgan, Dept Quim, Bellaterra 08193, Catalonia, Spain
[3] Inst Catal Nanotecnol, Nanobioelect & Biosensors Grp, Bellaterra, Catalonia, Spain
来源：
JOURNAL OF NANOPARTICLE RESEARCH | 2008年 / 10卷 / Suppl 1期
关键词：
Gold nanoparticles; Silver nanoparticles; Au-Ag nanoparticles; Ag-Au nanoparticles; Cyclic voltammetry; Colloids;
D O I：
10.1007/s11051-008-9374-3
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Simple strategies for producing silver and gold nanoparticles (AgNP and AuNP) along with the corresponding core shell nanoparticles (Au-Ag and Ag-Au) by reduction of the metal salts AgBF4 and HAuCl4 by NaBH4 in water will be presented. The morphologies of the obtained nanoparticles are determined by the order of addition of reactants. The obtained NPs, with sizes in the range 3-40 nm, are characterized by transmission electronic microscopy (TEM) and UV-Vis absorption spectroscopy, so as to evaluate their qualities. Moreover, a direct electrochemical detection protocol based on a cyclic voltammetry in water solution that involves the use of glassy carbon electrode is also applied to characterize the prepared NPs. The developed NPs and the related electroanalytical method seem to be with interest for future sensing and biosensing applications including DNA sensors and immunosensors.
引用
收藏
页码：97 / 106
页数：10
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