Optimization of sample preparation techniques for the determination of 4-nonylphenol in water and sediment

被引：11
|
作者：
Chee, KK
Wong, MK
Lee, HK
机构：
[1] Department of Chemistry, National University of Singapore
来源：
JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES | 1996年 / 19卷 / 02期
关键词：
D O I：
10.1080/10826079608005511
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
Sample preparation techniques for the determination of 4-nonylphenol in water and sediments were optimized using two-level orthogonal array design (OAD). Comparison between the use of cartridge-based solid-phase extraction and membranous disk-based extraction was made for water samples. For sediment samples, microwave-assisted solvent extraction (MASE) was employed. A comparison between MASE and classical soxhlet extraction of spiked samples was also carried out. 4-Nonylphenol was determined using high performance liquid chromatography (HPLC) coupled to both ultraviolet and fluorescence detection.
引用
收藏
页码：259 / 275
页数：17
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