Two new guaianolide-type sesquiterpenoids from Kadsura interior

被引：9
|
作者：
Dong, Ke [1 ]
Pu, Jian-Xin [1 ]
Du, Xue [1 ]
Li, Xiao-Nian [1 ]
Sun, Han-Dong [1 ]
机构：
[1] Chinese Acad Sci, Kunming Inst Bot, State Key Lab Phytochem & Plant Resources West Ch, Kunming 650204, Peoples R China
来源：
CHINESE CHEMICAL LETTERS | 2013年 / 24卷 / 02期
关键词：
Kadsura interior; 4 beta,9 beta-Dihydroxy-1 alpha,5 alpha-H-guaia-6,10(14)-dien; 4; beta; 9; 10; alpha-Trihydroxy-1; alpha; 5; alpha-H-guaia; 6-en; X-ray technique; LIGNANS;
D O I：
10.1016/j.cclet.2013.01.024
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Two new guaianolide-type sesquiterpenoids, 4 beta,9 beta-dihydroxy-1 alpha,5 alpha-H-guaia-6,10(14)-dien (1) and 4 beta,9 beta,10 alpha-trihydroxy-1 alpha,5 alpha-H-guaia-6-en (2), along with four known sesquiterpenoids (3a, 3b, 4 and 5), were isolated from Kadsura interior. Their structures and configurations were elucidated by spectroscopic methods including 2D-NMR and HR-MS techniques. Compounds 3a and 3b were obtained as a pair of enantiomers, and their structure and absolute configuration were established from their extensive NMR spectra and by single-crystal X-ray analysis. (C) 2013 Jian-Xin Pu. Published by Elsevier B.V. on behalf of Chinese Chemical Society. All rights reserved.
引用
收藏
页码：111 / 113
页数：3
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