Low-temperature synthesis of nano-crystalline MgTi2O5 powders by aqueous Sol-Gel process

被引:3
|
作者
Chen, X. F. [1 ]
Li, J. [1 ]
Feng, T. T. [1 ]
Jiang, Y. S.
Zhang, X. H. [1 ]
Wu, H. T. [1 ]
Yue, Y. L. [1 ]
机构
[1] Univ Jinan, Sch Mat Sci & Engn, Shandong Prov Key Lab Preparat & Measurement Bldg, Jinan 250022, Peoples R China
来源
关键词
MgTi2O5; Nanopowder Synthesis; Aqueous Sol-Gel Process; MAGNESIUM TITANATE; PURE MGTIO3;
D O I
10.4028/www.scientific.net/KEM.538.177
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The pseudobrookite-structure MgTi2O5 was successfully synthesized by the aqueous sol-gel method using titanium dioxide and magnesium nitrate as starting materials instead of expensive organic solvent and metal alkoxides. The as-prepared nanopowders were characterized by X-ray diffraction (XRD), differential thermal analysis (DTA) and transmission electron microscope (TEM), respectively. The results showed that the calcinations process of gel consisted of a series of oxidation and combustion reactions, accompanied by significantly exothermal effects. Highly reactive nanosized magnesium titanate powders were successfully obtained at 650 degrees C with less than similar to 100 nm.
引用
收藏
页码:177 / 180
页数:4
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