Methods of assaying volatile oxygenated organic compounds in effluent samples by gas chromatography-A review

被引：61

作者：

Makos, Patrycja ^{[1
]}

Przyjazny, Andrzej ^{[2
]}

Boczkaj, Grzegorz ^{[1
]}

机构：

[1] Gdansk Univ Technol, Fac Chem, Dept Proc Engn & Chem Technol, G Narutowicza St 11-12, PL-80233 Gdansk, Poland

[2] Kettering Univ, Dept Chem & Biochem, 1700 Univ Ave, Kettering Flint, MI 48504 USA

来源：

JOURNAL OF CHROMATOGRAPHY A | 2019年 / 1592卷

关键词：

Derivatization; Effluents; Extraction; Gas chromatography; Sample preparation; Volatile organic compounds; SOLID-PHASE MICROEXTRACTION; LIQUID-LIQUID MICROEXTRACTION; WASTE-WATER TREATMENT; VACUUM-ULTRAVIOLET SPECTROSCOPY; INJECTION-PORT DERIVATIZATION; ADVANCED OXIDATION PROCESSES; IONIZATION MASS-SPECTROMETRY; SINGLE-DROP MICROEXTRACTION; BASIC PH CONDITIONS; CHAIN FATTY-ACIDS;

D O I：

10.1016/j.chroma.2019.01.045

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

The paper is a review of the procedures for the determination of volatile and semivolatile oxygenated organic compounds (O-VOCS) in effluent samples by gas chromatography. Current trends and outlook for individual steps of the procedure for the determination of O-VOCs in effluents are discussed. The available sample preparation techniques and their limitations are described along with GC capillary columns used for O-VOCs separation and selective and universal detectors used for their determination. The results of determination of O-VOC content in various types of real effluents are presented. The lack of legal regulations regarding the presence of the majority of O-VOCs is pointed out as well as the availability of just a few procedures allowing a comprehensive evaluation of the O-VOC content in effluents. (C) 2019 Elsevier B.V. All rights reserved.

引用

页码：143 / 160

页数：18

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