Microwave-Assisted Synthesis of Poly(Aspartic Acid-Itaconic Acid) Copolymer and Its Characterization

被引：0

作者：

Zhang Yuling ^{[1
]}

Jiang Yijian ^{[1
]}

Hu Zhiguang ^{[1
]}

Wei Hanxiao ^{[1
]}

Guo Jun ^{[2
]}

Wang Jilong ^{[1
]}

机构：

[1] North China Elect Power Univ, Dept Environm Engn Sci, Baoding 071003, Peoples R China

[2] North China Elect Power Univ, Dept Comp, Baoding 071003, Peoples R China

来源：

CHINA PETROLEUM PROCESSING & PETROCHEMICAL TECHNOLOGY | 2016年 / 18卷 / 03期

基金：

中国国家自然科学基金;

关键词：

aspartic acid; itaconic acid; copolymerization; scale inhibition; POLYASPARTIC ACID; SCALE INHIBITION;

D O I：

暂无

中图分类号：

TE [石油、天然气工业]; TK [能源与动力工程];

学科分类号：

0807 ; 0820 ;

摘要：

Poly(aspartic acid-itaconic acid) copolymer was synthesized from aspartic acid (Asp) and itaconic acid (Ita) under microwave irradiation. The effects of microwave power, microwave irradiation time, molar ratio of itaconic acid and aspartic acid, catalyst type, catalyst and organic solvent content on copolymer yield, and the performance for inhibition of CaCO3 fouling were investigated. It was found that the product yield achieved a highest record of 95% when the amount of catalyst NaH2PO4 was 0.012 mol, the amount of organic solvent propylene carbonate was 16 mL, the molar ratio of Asp/Ita was 3: 1, the microwave output power was 1200 W and the irradiation time was 5.5 min. And the product performance for inhibition of calcium carbonate also reached a highest value of 94.38%. Structural characterization of the product showed that the product was the aspartic acid-itaconic acid copolymer.

引用

页码：76 / 82

页数：7

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