In-situ synthesis of palladium nanoparticles-filled carbon nanotubes using arc-discharge in solution

被引：77
|
作者：
Bera, D
Kuiry, SC
McCutchen, M
Kruize, A
Heinrich, H
Meyyappan, M
Seal, S
机构：
[1] Univ Cent Florida, Adv Mat Proc & Analysis Ctr, Orlando, FL 32816 USA
[2] Univ Groningen, Mat Sci Grp, Dept Appl Phys, NL-9747 AG Groningen, Netherlands
[3] NASA, Ames Res Ctr, Ctr Nanotechnol, Moffett Field, CA 94035 USA
来源：
CHEMICAL PHYSICS LETTERS | 2004年 / 386卷 / 4-6期
基金：
美国国家科学基金会;
关键词：
D O I：
10.1016/j.cplett.2004.01.082
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
A unique, simple, inexpensive and one-step synthesis route of carbon nanotubes (CNT) supported palladium nanoparticles using a simplified arc-discharge in solution is reported. Palladium nanoparticles with 3 nm diameter were found to form during reduction of palladium tetra-chloro-square-planar complex. Pd-nanoparticles were simultaneously encapsulated in CNTs during the rolling of graphene sheets in the arc-discharge process. Energy Dispersive Spectroscopy suggests no functionalization of chlorine to the sidewall of CNTs. Study of High Resolution Transmission Electron microscopy supports the scroll mechanism for CNT formation. (C) 2004 Elsevier B.V. All rights reserved.
引用
收藏
页码：364 / 368
页数：5
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