Synthesis of Nickel Nanoparticles Via Non-Aqueous Polyol Method: Effect of Reaction Time

被引：0
|
作者：
Roselina, N. R. Nik [1 ]
Azizan, A. [2 ]
Lockman, Z. [2 ]
机构：
[1] Univ Teknol MARA UiTM Shah Alam, Fac Mech Engn, Shah Alam 40450, Selangor, Malaysia
[2] Univ Sains Malaysia, Sch Mat & Mineral Resources Engn, Nibong Tebal 14300, Pulau Pinang, Malaysia
来源：
SAINS MALAYSIANA | 2012年 / 41卷 / 08期
关键词：
Nanoparticles; nickel; polyol; NANOPOWDERS; SIZE;
D O I：
暂无
中图分类号：
O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];
学科分类号：
07 ; 0710 ; 09 ;
摘要：
This paper presents facile and rapid synthesis route of Ni nanoparticles at approximately 180 degrees C in the mixture composed of ethylene glycol (EG) with hydrazine (N2H4) as a reducing agent. X-ray diffraction (XRD) analysis revealed that Ni2+ can be reduced completely to Ni metal in 15 min. XRD analysis also indicated that the as-synthesized nanoparticles were pure Ni with face-centered cubic (fcc) crystal structure. Transmission electron microscopy (TEM) results showed that the sample with heating duration of 15 min has the most narrow size distribution and the size increased as the reaction time increased.
引用
收藏
页码：1037 / 1042
页数：6
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