Differentiation of Turkish Rakies through Headspace Solid-Phase Microextraction and Gas Chromatography-Mass Spectrometry Analysis

被引:5
|
作者
Yilmaztekin, M. [1 ]
Cabaroglu, T. [2 ]
Gunata, Z. [3 ]
机构
[1] Inonu Univ, Dept Food Engn, Fac Engn, TR-44280 Malatya, Turkey
[2] Cukurova Univ, Dept Food Engn, Fac Agr, TR-01330 Adana, Turkey
[3] Univ Montpellier 2, UMR Qualisud, F-34095 Montpellier 5, France
关键词
anethole; estragole; gas chromatography-mass spectrometry; PCA; solid-phase microextraction; Turkish raki; METHANOL; AROMA;
D O I
10.1002/j.2050-0416.2011.tb00513.x
中图分类号
TS2 [食品工业];
学科分类号
0832 ;
摘要
J. Inst. Brew. 117(4), 622-626, 2011 Composition of flavour compounds from several commercial raki samples was determined through headspace solid-phase microextraction (HS-SPME) and gas chromatography coupled to mass spectrometry (GC MS). The extraction of volatile compounds was performed using a 75 mu m CAR/PDMS fibre. Forty three volatile compounds were identified. The major compounds were trans-anethole (86.47-94.19%), valencene (1.15-6.77%), estragole (2.66-5.46%), and cis-anethole (0.72-2.33%). Principal component analysis (PCA) enabled the differentiation of the raki samples thanks to compounds arising mainly from aniseed.
引用
收藏
页码:622 / 626
页数:5
相关论文
共 50 条
  • [1] Analysis of cannabis material by headspace solid-phase microextraction combined with gas chromatography-mass spectrometry
    Ilias, Y
    Rudaz, S
    Mathieu, P
    Veuthey, JL
    Christen, P
    [J]. CHIMIA, 2004, 58 (04) : 219 - 221
  • [2] Automated headspace solid-phase microextraction versus headspace for the analysis of furan in foods by gas chromatography-mass spectrometry
    Altaki, M. S.
    Santos, F. J.
    Galceran, M. T.
    [J]. TALANTA, 2009, 78 (4-5) : 1315 - 1320
  • [3] Determination of oxadiazon residues by headspace solid-phase microextraction and gas chromatography-mass spectrometry
    Navalón, A
    Prieto, A
    Araujo, L
    Vílchez, JL
    [J]. JOURNAL OF CHROMATOGRAPHY A, 2002, 946 (1-2) : 239 - 245
  • [4] Speciation of inorganic and tetramethyltin by headspace solid-phase microextraction and gas chromatography-mass spectrometry
    Tzollas, Nikolaos M.
    Zachariadis, George A.
    [J]. JOURNAL OF SEPARATION SCIENCE, 2010, 33 (11) : 1610 - 1616
  • [5] Analysis of benzothiazole in Italian wines using headspace solid-phase microextraction and gas chromatography-mass spectrometry
    Bellavia, V
    Natangelo, M
    Fanelli, R
    Rotilio, D
    [J]. JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2000, 48 (04) : 1239 - 1242
  • [6] Headspace solid-phase microextraction and gas chromatography-mass spectrometry analysis of free volatile compounds inMango
    Chunqing Shang
    Chunhui Deng
    Xiaoyue Zhang
    Zhengfu Chen
    Yaoming Hu
    [J]. Chromatographia, 2002, 55 : 737 - 741
  • [7] Enantiomeric Analysis of Flavor Compounds by Multiple Headspace Solid-Phase Microextraction Gas Chromatography-Mass Spectrometry
    Saito, Koichi
    Oshiro, Yukino
    Sakata, Osamu
    Ito, Rie
    [J]. CHROMATOGRAPHY, 2019, 40 (03) : 105 - 114
  • [8] Headspace Solid-Phase Microextraction and Gas Chromatography-Mass Spectrometry for Analysis of VOCs Produced by Phytophthora cinnamomi
    Qiu, Rui
    Qu, Dong
    Trengove, Robert
    Agarwal, Manjree
    Hardy, Giles E. St J.
    Ren, Yonglin
    [J]. PLANT DISEASE, 2014, 98 (08) : 1099 - 1105
  • [9] Headspace solid-phase microextraction and gas chromatography-mass spectrometry analysis of free volatile compounds in Mango
    Shang, CQ
    Deng, CH
    Zhang, XY
    Chen, ZF
    Hu, YM
    [J]. CHROMATOGRAPHIA, 2002, 55 (11-12) : 737 - 741
  • [10] ANALYSIS OF CIGARETTE SMOKE BY HEADSPACE SOLID PHASE MICROEXTRACTION GAS CHROMATOGRAPHY-MASS SPECTROMETRY
    Yang, Qiong
    Tuo, Suxing
    Zhao, Yu
    Wei, Weiwei
    Huang, Yongbing
    Chen, Bo
    Yang, Huawu
    [J]. ANALYTICAL LETTERS, 2014, 47 (12) : 1995 - 2002