Spectroturbidimetric Determination of the Size, Concentration, and Refractive Index of Silica Nanoparticles

被引:5
|
作者
Khlebtsov, B. N. [1 ]
Khanadeev, V. A. [2 ]
Khlebtsov, N. G. [1 ,2 ]
机构
[1] Russian Acad Sci, Inst Biochem & Physiol Plants & Microorganisms, Saratov 410049, Russia
[2] Saratov NG Chernyshevskii State Univ, Saratov 410026, Russia
基金
俄罗斯基础研究基金会;
关键词
D O I
10.1134/S0030400X08110143
中图分类号
O43 [光学];
学科分类号
070207 ; 0803 ;
摘要
A method for determining the refractive index, size, and concentration of silica nanoparticles used as cores in synthesis of gold nanoshells is described. The average refractive index of silica nanoparticles, n = 1.475 +/- 0.005, is determined by a modified immersion method, which involves spectroturbidimetry data in immersion media (dimethyl sulfoxide + ethanol). Working calibrations are obtained, which allow one to determine the size and concentration of silica particles and, correspondingly, the concentration of gold nanoshells in final preparations from measured values of the wavelength exponent and optical density.
引用
收藏
页码:732 / 738
页数:7
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