Determination of Formaldehyde in Romanian Cosmetic Products using Coupled GC/MS System after SPME Extraction

被引：2
|
作者：
Feher, I. [1 ]
Schmutzer, G. [1 ]
Voica, C. [1 ]
Moldovan, Z. [1 ]
机构：
[1] Natl Inst Res & Dev Isotop & Mol Technol, Cluj Napoca 400293, Romania
来源：
PROCESSES IN ISOTOPES AND MOLECULES (PIM 2013) | 2013年 / 1565卷
关键词：
formaldehyde determination; cosmetic products; SPME extraction; GC/MS analysis; SOLID-PHASE MICROEXTRACTION;
D O I：
10.1063/1.4833748
中图分类号：
O59 [应用物理学];
学科分类号：
摘要：
In this study we have made a quick review of some Romanian cosmetic products (shampoo, conditioner, face wash) in order to determine the formaldehyde content as well as other substances called "formaldehyde releasers". The process was performed based on solid-phase microextraction (SPME) followed by gas chromatography/mass spectrometry technique. Prior to SPME extraction we used a derivation step of formaldehyde using pentafluorophenyl hydrazine. The obtained product was adsorbed on SPME devices, then injected and desorbed into the GC/MS injection port. The concentration of formaldehyde (as derived compound) was calculated using calibration curve, having a regression coefficient of 0.9938. The performance parameters of the method were calculated using samples of standard concentration. The method proved to be sensitive, having a quantification limit (LOQ) of 0.15 mu g/g.
引用
收藏
页码：294 / 297
页数：4
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