One-pot preparations of (dichloroiodo)arenes from some arenes

被引：6
|
作者：
Lulinski, P [1 ]
Obeid, N [1 ]
Skulski, L [1 ]
机构：
[1] Med Univ, Fac Pharm, Chair & Lab Organ Chem, PL-02097 Warsaw, Poland
来源：
BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN | 2001年 / 74卷 / 12期
关键词：
D O I：
10.1246/bcsj.74.2433
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Arenes (ArH) were substituted with some transient I3+ species, generated in situ in appropriate, anhydrous I-2/NaIO4 or NaIO3/AcOH/AC(2)O/Concd H2SO4 mixtures, to form soluble organoiodine(III) intermediates, ArISO4, Next, excess coned hydrochloric acid was added to precipitate out the title ArICI2, and isolated in 46-88% optimized crude yields.
引用
收藏
页码：2433 / 2434
页数：2
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