Synthesis and Performance of NaA/MCM-48 Micro-mesoporous Composite Molecular Sieve

被引:0
|
作者
Pan, Jianmin [1 ]
Cheng, Yue
Wei, Yunyang [1 ]
机构
[1] Nanjing Univ Sci & Technol, Sch Chem Engn, Nanjing 210094, Jiangsu, Peoples R China
来源
关键词
NaA/MCM-48; micro-mesoporous; molecular sieve; hydrothermal synthesis; cationic red X-5GN; adsorption;
D O I
10.4028/www.scientific.net/AMR.476-478.1979
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
NaA/MCM-48 micro-mesoporous molecular sieve was prepared at 100 degrees C for 72 h by hydrothermal synthesis method, where chemicals with a equivalent ratio of n (SiO2):n (CTAB) :n (H2O) :n (NaOH) is 1:0.45:60:0.48 were added to NaA microporous molecular sieve prepared hydrothermally at 100 degrees C for 5 h from a composite solution with a equivalent ratio of Na2O:SiO2:Al2O3:H2O is 3:2:1 : 200. The adsorption of the NaA/MCM-48 micro-mesoporous molecular sieve to cationic red X-5GN simulated dye existing in the waste water showed that, in 50 mL of 20 mg/L cationic red X-5GN solution, under the optimal conditions of a dosage of NaA/MCM-48 micro-mesoporous composite molecular sieve of 1.8g/L, a pH of 7 and an oscillation time of 30min, the decoloration rate of spent solution was above 82.5%. The XRD, SEM and TEM processes were adopted for its characterization to display the possible reasons.
引用
收藏
页码:1979 / 1986
页数:8
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