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Hydrothermal synthesis and magnetic property of Cu3(OH)2V2O7•nH2O
被引:16
|作者:
Ni, Shibing
[1
]
Wang, Xinghui
[1
]
Zhou, Guo
[1
]
Yang, Feng
[1
]
Wang, Junming
[1
]
He, Deyan
[1
]
机构:
[1] Lanzhou Univ, Dept Phys, Lanzhou 730000, Peoples R China
关键词:
Nanocomposites;
Copper vanadium oxide hydroxide hydrate;
Microstructure;
Magnetic property;
ROOM-TEMPERATURE SYNTHESIS;
CRYSTAL-STRUCTURE;
ZINC PYROVANADATE;
X-RAY;
D O I:
10.1016/j.matlet.2009.11.063
中图分类号:
T [工业技术];
学科分类号:
08 ;
摘要:
Copper vanadium oxide hydroxide hydrate (Cu-3(OH)2V(2)O(7)center dot nH(2)O) nanoparticles with mean size of about 100 nm were successfully synthesized by a simple hydrothermal method. The structure and morphology of the as-synthesized products were characterized by X-ray diffraction (XRD), Field emission scanning electron microscopy (FE-SEM), Raman spectra, and Fourier transform infrared spectra (FTIR). The composition and purity of the as-synthesized Cu-3(OH)2V(2)O(7)center dot nH(2)O nanoparticles were characterized by Energy disperse spectroscopy (EDS) and X-ray photoelectron spectroscopy (XPS). The magnetic property of the as synthesized Cu-3(OH)2V(2)O(7)center dot nH(2)O nanoparticles was characterized by vibrant sample magnetometer. Magnetic hysteresis curve indicate that the as-synthesized nanoparticles are of weak ferromagnetic property at room temperature. (C) 2009 Elsevier B.V. All rights reserved.
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页码:516 / 519
页数:4
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