Synthesis of nanostructured and microstructured ZnO and Zn(OH)2 on activated carbon cloth by hydrothermal and microwave-assisted chemical bath deposition methods

被引:10
|
作者
Mosayebi, Elham [1 ]
Azizian, Saeid [1 ]
Hajian, Ali [1 ]
机构
[1] Bu Ali Sina Univ, Dept Phys Chem, Fac Chem, Hamadan, Iran
关键词
Microstructure; Crystal structure; Nano crystalline materials; CRYSTALLINE ZNO; NANOROD ARRAYS; NANOBELT; GROWTH; FILM;
D O I
10.1016/j.spmi.2014.12.039
中图分类号
O469 [凝聚态物理学];
学科分类号
070205 ;
摘要
Nanostructured and microstructured ZnO and Zn(OH)(2) loaded on activated carbon cloth were synthesized by microwave-assisted chemical bath deposition and hydrothermal methods. By hydrothermal method the deposited sample on carbon fiber is pure ZnO with dandelion-like nanostructures. By microwave-assisted chemical bath method the structure and composition of deposited sample depends on solution pH. At pH = 9.8 the deposited sample on carbon fiber is pure ZnO with flower-like microstructure; but at pH = 10.8 the sample is a mixture of ZnO and Zn(OH)(2) with flower-like and rhombic microstructures, respectively. The mechanism of crystal grow by microwave-assisted chemical bath method was investigated by SEM method at both pH. (C) 2015 Elsevier Ltd. All rights reserved.
引用
收藏
页码:226 / 232
页数:7
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