Structural, optical, electrical and magnetic properties of aluminum substituted Co-Cu-Zn nano-crystalline ferrites

被引:2
|
作者
Trinadh, B. [1 ,2 ]
Suresh, J. [3 ]
Patta, G. R. [4 ]
Babu, K. Vijaya [5 ]
Komali, Ch [6 ]
Babu, B. Vikram [7 ]
Devi, K. Anjani [8 ]
Mohan, B. Sathish [9 ]
Samatha, K. [1 ]
机构
[1] Andhra Univ, Dept Phys, Visakhapatnam 530003, Andhra Prades, India
[2] GVSM Govt Degree Coll, Ulavapadu 523292, Andhra Pradesh, India
[3] BVC Coll Engn, Dept Phys, Rajamahendravaram 533102, Andhra Pradesh, India
[4] Rajiv Gandhi Univ Knowledge Technol, Dept Phys, Srikakulam 532402, Andhra Pradesh, India
[5] Ctr Univ Technol & Management, Dept Phys, Vizianagaram 535003, India
[6] Anil Neerukonda Inst Technol & Sci, Dept Phys, Visakhapatnam 531162, Andhra Pradesh, India
[7] Int Sch Technol & Sci ISTS Women, Dept Phys, Rajamahendravaram 533294, Andhra Pradesh, India
[8] Aditya Engn Coll, Dept Phys, Surampalem 533437, India
[9] Bio Enviro Chem Solut, Visakhapatnam 530017, India
关键词
Spinel ferrite; Crystallite size; Dielectric loss; Coercivity; Loss tangent; DIELECTRIC-PROPERTIES; NANOPARTICLES;
D O I
10.1016/j.ssc.2023.115360
中图分类号
O469 [凝聚态物理学];
学科分类号
070205 ;
摘要
Strong electrical resistivity, low eddy current and dielectric losses, high saturation magnetization, high perme-ability, and other significant electrical and magnetic properties of nano-ferrites are only a few. In this investi-gation a sincere effort has been tried to manufacture Co0.7Cu0.2Zn0.1Fe2-xAlxO4 (x = 0, 0.02, 0.04, 0.06, 0.08, 0.10) nano-ferrites utilizing sol-gel auto-combustion process and systematically characterize the structural, op-tical, electrical and magnetic features. All the peaks belonging to XRD confirmed a structure of the spinel class and single phase with zero impurities. The intensity ratios are generated for a number of cation combinations occupying tetrahedral and octahedral B site. The higher band (nu 1) is identified in between wave numbers 550-600 cm-1 as a result of the vibrations of stretching pertaining to the metal-oxygen tetrahedral band. The grain sizes are measured by the use of image J software associated with the SEM, which are indicated on the images in the range of 3.14 mu m-1.215 mu m. With a frequency-independent characteristic, the dielectric loss dwindles quickly at low frequencies and slows down at high frequencies. Because of spin non-collinearity at the crystal's surface, the saturation magnetization values climb as particle sizes increase. The coercivity values gradually decline as aluminum concentration rises.
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页数:9
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