Preparation, Characterization, and Antibacterial Activity of Silver Nanoparticle-Decorated Ordered Mesoporous Carbon

被引:0
|
作者
Nguyen, Dung Van [1 ]
Nguyen, Duong Thuy [1 ]
Tran, Vi Le Tuong [1 ]
Vo, Khang Dinh [1 ]
Nguyen, Long Quang [1 ]
机构
[1] VNU HCM, Ho Chi Minh City Univ Technol HCMUT, Fac Chem Engn, Ho Chi Minh City, Vietnam
关键词
mesoporous carbon; soft template; silver nanoparticles; green synthesis; antibacterial activity; Staphylococcus aureus; GREEN; AG;
D O I
10.48084/etasr.5782
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
In this study, Ordered Mesoporous Carbon (OMC) was prepared using resol as a carbon precursor and F127 as a soft template. Small-angle X-ray Diffraction (XRD), Transmission Electron Microscopy (TEM) images, and nitrogen adsorption and desorption isotherms revealed that OMC possessed ordered hexagonal mesostructures (p6m) with an ordered pore size of 3.2nm, a high specific surface area (S-BET) of 539m(2) /g, and a large total pore volume (V-total) of 0.44cm(3) /g. Subsequently, silver nanoparticles synthesized from an aqueous AgNO3 solution using glucose as a reducing agent and starch as a stabilizing agent were decorated on OMC, producing Ag/OMC. XRD analysis revealed that the composite contained silver crystals. In addition, the content and size of silver nanoparticles in Ag/OMC were 0.71wt% (AAS) and around 25-50nm (TEM), respectively. Due to the surface cover of silver nanoparticles, S-BET and V-total of Ag/OMC slightly decreased to 417m(2)/g and 0.38cm(3)/g, respectively. Both agar and broth dilution techniques were used to evaluate the antibacterial activity of the material against Staphylococcus aureus. Ag/OMC with a Minimum Inhibitory Concentration (MIC) of 25.0 mu g/mL is a potential candidate for use against Staphylococcus aureus.
引用
收藏
页码:10828 / 10833
页数:6
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