Synthesis and crystal structure of (S,E)-4-hydroxy-3-(2-((4aR,6aS,7R,10aS,10bR)-3,3,6a,10b-tetramethyl-8-methylenedecahydro-1H-naphtho[2,1-d][1,3]dioxin-7-yl)ethylidene)dihydrofuran-2(3H)-one, C23H34O5

被引:0
|
作者
Li, Shi-Qing [1 ]
Zhou, Jian [2 ]
Dong, Zhang-Chao [1 ]
Pan, Bo Wen [1 ]
Shi, Yang [1 ]
Zhou, Ying [1 ]
机构
[1] Guizhou Univ Tradit Chinese Med, Guiyang 550025, Peoples R China
[2] East China Normal Univ, Shanghai Engn Res Ctr Mol Therapeut & New Drug Dev, Shanghai Key Lab Green Chem & Chem Proc, Shanghai 200062, Peoples R China
关键词
2254956;
D O I
10.1515/ncrs-2023-0179
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
C23H34O5, orthorhombic, P2(1)2(1)2(1) (no. 19), a = 11.1838(3) angstrom, b = 11.7824(3) angstrom, c = 16.3160(5) angstrom, V = 2149.99(10) angstrom(3), Z = 4, R-gt(F) = 0.0399, wR(ref)(F-2) = 0.1097, T = 293 K.
引用
收藏
页码:735 / 737
页数:3
相关论文
共 50 条
  • [1] (2S,4aR,6aR,7R,9S,10aS,10bR)-7-Carboxy-2-(3-furyl)-6a,10b-dimethyl-4,10-dioxoperhydrobenzo[f]isochromen-9-yl acetate
    Carvalho, Paulo
    Kutrzeba, Lukasz M.
    Zjawiony, Jordan K.
    Avery, Mitchell A.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O471 - U1366
  • [2] Crystal structure of (3aR,4′R,7R,7aS)-tetrahydro-7-hydroxy-2,2,2′2′-tetramethylspiro[1,3-benzodioxole-5 (4H),4′-[1,3]dioxolan]-5′-one, C13H20O6
    Kelling, A
    Schilde, U
    Sefkow, M
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2000, 215 (04): : 513 - 514
  • [3] (7R,8S,10bR)-7,8-dihydroxy-1,5,6,7,8,9,10,10b-octahydro-3H-1, 3-oxazolo[4,3-a]isoquinolin-3-one
    Abboud, Khalil A.
    Butora, Gabor
    Fearnley, Stephen P.
    Gum, Andrew G.
    Stabile, Michele R.
    Hudlicky, Tomas
    Acta Crystallographica, Section C: Crystal Structure Communications, 1998, 54 (pt 8): : 1162 - 1164
  • [4] Crystal structures of 1∞{[Cd(phen)](C6H8O4)3/3} and 1∞{[Cd(phen)](C7H10O4)3/3} • 2H2O with C6H10O4 = adipic acid and C7H12O4 = pimelic acid
    Zheng, YQ
    Liu, WH
    Lin, JL
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2002, 628 (06): : 1401 - 1405
  • [5] (7R,8S,10bR)-7,8-dihydroxy-1,5,6,7,8,9,10,10b-octahydro-3H-1,3-oxazolo[4,3-a]isoquinolin-3-one
    Abboud, KA
    Butora, G
    Fearnley, SP
    Gum, AG
    Stabile, MR
    Hudlicky, T
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1998, 54 : 1162 - 1164
  • [6] Synthesis and Crystal Structure of Ethyl 2-(6-(1,3-Dioxo-4,5,6,7-tetrahydro-1H-isoindol-2(3H)-yl)-7-fluoro-3-oxo-2H-benzo[b][1,4]oxazin-4(3H)-yl) Butanoate
    吴道新
    罗斐贤
    莫洪波
    王晓光
    任叶果
    SIMPSON Jim
    黄明智
    结构化学, 2009, 28 (05) : 585 - 589
  • [7] Synthesis and Crystal Structure of Ethyl 2-(6-(1,3-Dioxo-4,5,6,7-tetrahydro-1H-isoindol-2(3H)-yl)-7-fluoro-3-oxo-2H-benzo[b][1,4]oxazin-4(3H)-yl) Butanoate
    Wu Dao-Xin
    Luo Fei-Xian
    Mo Hong-Bo
    Wang Xiao-Guang
    Ren Ye-Guo
    Simpson, Jim
    Huang Ming-Zhi
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2009, 28 (05) : 585 - 589
  • [8] Synthesis and Crystal Structure of Ethyl 2-(6-(1,3-Dioxo-4,5,6,7-tetrahydro-1H-isoindol-2(3H)-yl)-7-fluoro-3-oxo-2H-benzo[b][1,4]oxazin-4(3H)-yl) Butanoate
    吴道新
    罗斐贤
    莫洪波
    王晓光
    任叶果
    SIMPSON Jim
    黄明智
    Chinese Journal of Structural Chemistry, 2009, 28 (05) : 585 - 589
  • [9] Different coordination modes of 3-hydroxy-1,2,3-benzotriazin-4(3H)-one:: Molecular structures of (μ-H)Os3(CO)10(μ2-(2,3-η2)-(O)NNNC7H4O) and (μ-H)Ru3(CO)10(μ2-(1,2-η2)-NNN(O)C7H4O)
    Kumaresan, S
    Lu, KL
    Hung, JT
    Lee, FY
    Wen, YS
    Hwu, JR
    JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1997, 549 (1-2) : 155 - 161
  • [10] Crystal structure of (1S,3aR,3bR,10aR,10bR,12aR)-8-amino-3a,3b,6,6,10a-pentamethyl-1-((S)-2,6,6-trimethyltetrahydro-2H-pyran-2-yl)-2,3,3a, 3b, 4,5,5a, 6,10,10a, 10b, 11,12,12a-tetradecahydro-1H-cyclopenta[7,8] phenanthro[2,3-d]thiazol-12-ol - a panaxadiol dervative, C31H50N2O2S
    Wang, Jia-Zhen
    Weng, Wei-Zhao
    Ma, Ying
    He, Xiu-Ting
    Meng, Qing-Guo
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2019, 234 (03): : 397 - 400