Synthesis and post-polymerization modification of poly(diglycidyl fumarate)s and their thermal properties

被引：0
|
作者：
Mori, Yasuyuki [1 ,2 ]
Tada, Ryu [2 ]
Okano, Ippei [3 ]
Tamaso, Ken-ichi [3 ]
Ogawa, Ryo [3 ]
Shinozuka, Toyofumi [3 ]
Furusho, Yoshio [1 ,2 ]
Endo, Takeshi [2 ]
机构：
[1] Shiga Univ Med Sci, Dept Fundamental Biosci, Div Chem, Otsu, Japan
[2] Shiga Univ Med Sci, Mol Engn Inst, Otsu, Shiga 5202192, Japan
[3] R&D Div, Funct Polymers Dev Lab, Saitama, Japan
来源：
JOURNAL OF POLYMER SCIENCE | 2024年 / 62卷 / 07期
关键词：
carbon dioxide; epoxy group; polyfumarates; post-polymerization modification; radical polymerization; 1,2-DISUBSTITUTED ETHYLENIC MONOMERS; RADICAL HIGH POLYMERIZATION; GASEOUS CARBON-DIOXIDE; POLY(DI-TERT-BUTYL FUMARATE); POLY(GLYCIDYL METHACRYLATE); POLY(FUMARIC ACID); COPOLYMERIZATION; OXIRANE; POLYMERS; BEARING;
D O I：
10.1002/pol.20230898
中图分类号：
O63 [高分子化学（高聚物）];
学科分类号：
070305 ; 080501 ; 081704 ;
摘要：
The radical polymerization of diglycidyl fumarates was performed to give the poly(fumarate)s bearing epoxy groups in the side chains. Their post-polymerization modification with carbon dioxide afforded the poly(fumarate)s containing the five-membered cyclic carbonate structures by the reaction of epoxy groups in the polymer side chains with carbon dioxide. Besides, the thermal stability and behavior of the obtained poly(fumarate)s were examined by thermogravimetric and differential scanning calorimetry analyses.
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页码：1460 / 1467
页数：8
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