A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell

被引：8

作者：

Husband, Rachel J. ^{[1
]}

Strohm, Cornelius ^{[1
]}

Appel, Karen ^{[2
]}

Ball, Orianna B. ^{[3
,4
]}

Briggs, Richard

Buchen, Johannes

Cerantola, Valerio ^{[2
,25
]}

Chariton, Stella ^{[7
]}

Coleman, Amy L. ^{[5
]}

Cynn, Hyunchae ^{[5
]}

Dattelbaum, Dana ^{[8
]}

Dwivedi, Anand ^{[2
]}

Eggert, Jon H. ^{[5
]}

Ehm, Lars ^{[2
,9
]}

Evans, William J. ^{[5
]}

Glazyrin, Konstantin

Goncharov, Alexander F. ^{[10
]}

Graafsma, Heinz ^{[1
]}

Howard, Alex ^{[11
,12
]}

Huston, Larissa

Hutchinson, Trevor M.

Hwang, Huijeong ^{[1
,26
]}

Jacob, Sony ^{[5
]}

Kaa, Johannes ^{[2
,13
]}

Kim, Jaeyong ^{[14
]}

Kim, Minseob ^{[11
,12
]}

Koemets, Egor ^{[6
]}

Konopkova, Zuzana ^{[2
]}

Langenhorst, Falko ^{[15
]}

Laurus, Torsten ^{[1
]}

Li, Xinyang ^{[1
,27
]}

Mainberger, Jona ^{[1
]}

Marquardt, Hauke ^{[6
]}

McBride, Emma E. ^{[16
,28
]}

McGuire, Christopher ^{[5
]}

McHardy, James D. ^{[3
,4
]}

McMahon, Malcolm I. ^{[3
,4
]}

McWilliams, R. Stewart ^{[3
,4
]}

Mendez, Alba S. J.

Mondal, Anshuman

Morard, Guillaume ^{[18
]}

O'Bannon, Earl F. ^{[5
]}

Otzen, Christoph ^{[15
,29
]}

Pepin, Charles M. ^{[19
,20
]}

Prakapenka, Vitali B. ^{[7
]}

Prescher, Clemens ^{[21
]}

Preston, Thomas R. ^{[2
]}

Redmer, Ronald ^{[22
]}

Roeper, Michael ^{[1
]}

Sanchez-Valle, Carmen ^{[17
]}

机构：

[1] Deutsch Elekt Synchrotron DESY, Notkestr 85, D-22607 Hamburg, Germany

[2] European XFEL, Holzkoppel 4, D-22869 Schenefeld, Germany

[3] Univ Edinburgh, SUPA, Sch Phys & Astron, Peter Guthrie Tait Rd, Edinburgh EH9 3FD, Midlothian, Scotland

[4] Univ Edinburgh, Ctr Sci Extreme Condit, Peter Guthrie Tait Rd, Edinburgh EH9 3FD, Midlothian, Scotland

[5] Lawrence Livermore Natl Lab, Phys & Life Sci Directorate, Livermore, CA 94550 USA

[6] Univ Oxford, Dept Earth Sci, South Parks Rd, Oxford OX1 3AN, England

[7] Univ Chicago, Consortium Adv Radiat Sources, 5640 South Ellis Ave, Chicago, IL 60637 USA

[8] Los Alamos Natl Lab, Shock & Detonat Phys M-9,PO 1663, Los Alamos, NM 87545 USA

[9] Dept Geosci, 255 Earth & Space Sci Bldg ESS, Stony Brook, NY 11794 USA

[10] Carnegie Sci Earth & Planets Lab, 5241 Broad Branch Rd NW, Washington, DC 20015 USA

[11] Washington State Univ, Dept Chem, Pullman, WA 99164 USA

[12] Inst Shock Phys, Pullman, WA 99164 USA

[13] Tech Univ Dortmund, Fak Phys DELTA, Maria Goeppert Mayer Str 2, D-44227 Dortmund, Germany

[14] Hanyang Univ, Dept Phys, 17 Haengdang Dong, Seoul 133791, South Korea

[15] Friedrich Schiller Univ Jena, Inst Geowissensch, Carl Zeiss Promenade 10, D-07745 Jena, Germany

[16] SLAC Natl Accelerator Lab, 2575 Sand Hill Rd, Menlo Pk, CA 94025 USA

[17] Univ Munster, Inst Mineral, Corrensstr 24, D-48149 Munster, Germany

[18] Univ Gustave Eiffel, Univ Grenoble Alpes, Univ Savoie Mont Blanc, CNRS,IRD,ISTerre, F-38000 Grenoble, France

[19] CEA, DAM, DIF, F-91297 Arpajon, France

[20] Univ Paris Saclay, Lab Mat Condit Extremes, CEA, F-91680 Bruyeres Le Chatel, France

[21] Albert Ludwigs Univ Freiburg, Inst Earth & Environm Sci, Hermann Herder Str 5, D-79104 Freiburg, Germany

[22] Univ Rostock, Inst Phys, Albert Einstein Str 23-24, D-18059 Rostock, Germany

[23] Argonne Natl Lab, High Pressure Collaborat Access Team HPCAT, Xray Sci Div XSD, 9700 S Cass Ave, Lemont, IL 60439 USA

[24] Deutsch GeoForschungsZentrum GFZ, Telegrafenberg, D-14473 Potsdam, Germany

[25] Univ Milano Bicocca, Dept Earth & Environm Sci DISAT, Piazza Scienza 4, I-20126 Milan, Italy

[26] Gwangju Inst Sci & Technol, Sch Earth Sci & Environm Engn, 123 Cheomdan Gwagiro, Gwangju 61005, South Korea

[27] Jilin Univ, Coll Phys, State Key Lab Superhard Mat, Changchun 130012, Peoples R China

[28] Queens Univ Belfast, Sch Math & Phys, Univ Rd, Belfast BT7 1NN, Antrim, North Ireland

[29] Albert Ludwigs Univ Freiburg, Inst Earth & Environm Sci, Hermann Herder Str 5, D-79104 Freiburg, Germany

[30] Univ Nevada, Nevada Extreme Condit Lab, 4505 S Maryland Pkwy, Las Vegas, NV 89154 USA

[31] X Spectrum GmbH, Luruper Hauptstr 1, D-22547 Hamburg, Germany

来源：

JOURNAL OF SYNCHROTRON RADIATION | 2023年 / 30卷

基金：

欧盟地平线“2020”; 英国科研创新办公室; 美国国家科学基金会; 欧洲研究理事会;

关键词：

extreme conditions science; X-ray free-electron lasers; diamond anvil cells; dynamic compression; EQUATION-OF-STATE; PHASE-DIAGRAMS; PRESSURE; NITROGEN; WATER; ICE; TRANSITION; RAMAN; GOLD; H2O;

D O I：

10.1107/S1600577523003910

中图分类号：

TH7 [仪器、仪表];

学科分类号：

0804 ; 080401 ; 081102 ;

摘要：

An experimental platform for dynamic diamond anvil cell (dDAC) research has been developed at the High Energy Density (HED) Instrument at the European X-ray Free Electron Laser (European XFEL). Advantage was taken of the high repetition rate of the European XFEL (up to 4.5 MHz) to collect pulse-resolved MHz X-ray diffraction data from samples as they are dynamically compressed at intermediate strain rates (<= 10(3) s(-1)), where up to 352 diffraction images can be collected from a single pulse train. The set-up employs piezo-driven dDACs capable of compressing samples in >= 340 mu s, compatible with the maximum length of the pulse train (550 mu s). Results from rapid compression experiments on a wide range of sample systems with different X-ray scattering powers are presented. A maximum compression rate of 87 TPa s(-1) was observed during the fast compression of Au, while a strain rate of similar to 1100 s(-1) was achieved during the rapid compression of N-2 at 23 TPa s(-1).

引用

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页码：671 / 685

页数：15

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