Investigation on Structural, Electrical and Dielectric Properties of Polyaniline/ZrO2 Composite

被引：0
|
作者：
Pattar, Jayadev [1 ]
Ashwini, I. S. [1 ]
Nagaraja, M. [2 ]
Chandra, S. Sarvesha [1 ]
Sreekanth, R. [3 ]
Mahendra, K. [1 ]
Manohara, S. R. [4 ]
机构：
[1] REVA Univ, Sch Appl Sci, Dept Phys, Bengaluru 560064, Karnataka, India
[2] Sri Siddhartha Acad Higher Educ, Dept Phys, SSIT, Tumakuru 572105, Karnataka, India
[3] REVA Univ, Sch Appl Sci, Dept Chem, Bengaluru 560064, Karnataka, India
[4] Siddaganga Inst Technol, Dept Phys, Nanocomposites & Mat Res Lab, Tumakuru 572103, Karnataka, India
来源：
POLYMER SCIENCE SERIES A | 2023年 / 65卷 / 06期
关键词：
CRYSTAL-STRUCTURE; CHARGE-TRANSPORT; PERFORMANCE; NANOCOMPOSITE; CONDUCTIVITY; RELAXATION; BEHAVIOR; FILMS; ZRO2;
D O I：
10.1134/S0965545X2460025X
中图分类号：
O63 [高分子化学（高聚物）];
学科分类号：
070305 ; 080501 ; 081704 ;
摘要：
The effect of ZrO2 nanoparticles on the structural, electrical, and dielectric properties of polyaniline was studied. ZrO2 nanoparticles with an average size of 8 nm were synthesized by a simple precipitation method and their tetragonal and monoclinic crystalline phase was confirmed. Polyaniline and its nanocomposite with ZrO2 have been synthesized by chemical oxidation method using CH3COOH as a doping agent and APS as an oxidant. The synthesized composites were analyzed by infrared spectroscopy, X-ray diffraction, scanning electronic microscopy, AC conductivity, dielectric and impedance spectroscopy. In Nyquist plots, systematic decrement in the semicircle size was observed with growth of ZrO2 content. The dielectric constant in the PANI/ZrO2 composite has been increased with an increase in weight content of ZrO2 in PANI matrix and exhibited the Maxwell-Wagner-Sillars effect.
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收藏
页码：813 / 821
页数：9
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