3-(5-Phenyl-2H-tetrazol-2-yl)pyridine

被引：0

作者：

Ershov, Ivan S. ^{[1
]}

Esikov, Kirill A. ^{[1
]}

Nesterova, Olga M. ^{[1
]}

Skryl'nikova, Mariya A. ^{[1
,2
]}

Khramchikhin, Andrey V. ^{[2
]}

Shmaneva, Nadezda T. ^{[1
]}

Chernov, Ivan S. ^{[1
]}

Chernova, Ekaterina N. ^{[3
]}

Puzyk, Aleksandra M. ^{[4
]}

Sivtsov, Eugene V. ^{[5
]}

Pavlyukova, Yuliya N. ^{[1
]}

Trifonov, Rostislav E. ^{[1
]}

Ostrovskii, Vladimir A. ^{[1
,3
]}

机构：

[1] Tech Univ, St Petersburg State Inst Technol, Dept Chem & Technol Nitrogen Containing Organ Cpds, 24-26-49 Moskovsky Ave, St Petersburg 190013, Russia

[2] Tech Univ, St Petersburg State Inst Technol, Dept Organ Chem, 24-26-49 Moskovsky Ave, St Petersburg 190013, Russia

[3] Russian Acad Sci, St Petersburg Fed Res Ctr, RAS, SPC, 39 14th Line, St Petersburg 199178, Russia

[4] St Petersburg State Univ, Res Pk,26 Universitetskii Prospect, St Petersburg 198504, Russia

[5] Tech Univ, St Petersburg State Inst Technol, Dept Phys Chem, 24-26-49 Moskovsky Ave, St Petersburg 190013, Russia

来源：

MOLBANK | 2023年 / 2023卷 / 01期

基金：

俄罗斯基础研究基金会;

关键词：

3-(5-phenyl-2H-tetrazol-2-yl)pyridine; synthesis; molecular structure; X-ray diffraction analysis; quantum chemistry calculation; NMR spectroscopy; IR spectroscopy; UV-Vis spectroscopy; mass spectrometry; quantum chemical calculation; BORONIC ACIDS; TETRAZOLES; ARYLATION;

D O I：

10.3390/M1598

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

3-(5-Phenyl-2H-tetrazol-2-yl)pyridine was synthesized by treating 5-phenyl-1H-tetrazole with pyridin-3-ylboronic acid under Chan-Evans-Lam coupling conditions. The structure and identity were confirmed by H-1, C-13-NMR spectroscopy, IR spectroscopy, UV-Vis spectroscopy, high-resolution mass spectrometry, and TLC. The molecular structure was studied experimentally by sequential X-ray diffraction analysis and theoretically by DFT B3LYP quantum chemistry calculation.

引用

页数：12

共 50 条

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