MgFe2O4@Tris magnetic nanoparticles: an effective and powerful catalyst for one-pot synthesis of pyrazolopyranopyrimidine and tetrahydrodipyrazolopyridine derivatives

被引:3
|
作者
Ramezaninejad, Zahra [1 ]
Shiri, Lotfi [1 ]
机构
[1] Ilam Univ, Fac Sci, Dept Chem, POB 69315516, Ilam, Iran
关键词
4-COMPONENT SYNTHESIS; PYRAZOLOPYRIDINES; EFFICIENT; MNPS;
D O I
10.1039/d3ra07934a
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Magnesium (Mg) as a metal has wide applications, but its use in chemical reactions is rarely reported. Currently, magnesium catalytic processes are being developed to synthesize basic chemical compounds. Therefore, an effective and recyclable nano-catalyst was synthesized using MgFe2O4@Tris in this study. The structure of MgFe2O4@Tris was characterized by various techniques including Fourier-transform infrared (FT-IR), scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy dispersive X-ray (EDX), thermogravimetric analysis (TGA), X-ray diffraction (XRD), and vibrating sample magnetometer (VSM) techniques. Finally, the catalytic activity of this nano-catalyst was evaluated for the synthesis of pyrazolopyranopyrimidine and tetrahydrodipyrazolopyridine derivatives. Among the advantages of this catalyst are its high catalytic activity, high yields, use of environmentally friendly solvents, easy magnetic separation, and the possibility of reusing the catalyst.
引用
收藏
页码:6006 / 6015
页数:10
相关论文
共 50 条
  • [1] Nano-CuCr2O4: an efficient catalyst for a one-pot synthesis of tetrahydrodipyrazolopyridine
    Shahbazi-Alavi, Hossein
    Safaei-Ghomi, Javad
    Eshteghal, Fahime
    Zahedi, Safura
    Nazemzadeh, Seyed Hadi
    Alemi-Tameh, Fatemeh
    Tavazo, Maryam
    Basharnavaz, Hadi
    Lashkari, Mohammad Rasool
    JOURNAL OF CHEMICAL RESEARCH, 2016, (06) : 361 - 363
  • [2] Synthesis of pyridodipyrimidine derivatives using MgFe2O4@Tris as a new nanocatalyst under green condition
    Ramezaninejad, Zahra
    Shiri, Lotfi
    RESEARCH ON CHEMICAL INTERMEDIATES, 2024, 50 (07) : 3135 - 3152
  • [3] One-pot synthesis of MgFe2O4 nanospheres by solvothermal method
    Shen, Yu
    Wu, Yanbo
    Li, Xinyong
    Zhao, Qidong
    Hou, Yang
    MATERIALS LETTERS, 2013, 96 : 85 - 88
  • [4] NiFe2O4 Nanoparticles: An Efficient Catalyst for One-Pot Three Component Synthesis of Acridinediones Derivatives
    Mhaske, A. K.
    Vikhe, D. V.
    Gadhave, A. G.
    Uphade, B. K.
    POLYCYCLIC AROMATIC COMPOUNDS, 2024,
  • [5] One-pot solvent-free synthesis of MgFe2O4 nanoparticles from ferrous sulfate waste
    Xiang, Hengli
    Peng, Xu
    Xu, Dehua
    Yang, Xiushan
    Ren, Genkuan
    Zhang, Zhiye
    Zhong, Yanjun
    Wang, Xinlong
    MATERIALS AND MANUFACTURING PROCESSES, 2020, 35 (05) : 590 - 597
  • [6] Microwave Synthesis of Fe2O3 Nanoparticles and Its Catalyst Investigation in One-pot Synthesis of Naphthoxazinone Derivatives
    Hashemzehi-Goonaki, A.
    Saffari, J.
    JOURNAL OF NANOSTRUCTURES, 2015, 5 (04) : 385 - 393
  • [7] Synthesis of 4H-pyran derivatives via a green one-pot multicomponent reaction catalyzed by CuFe2O4 magnetic nanoparticles as a reusable catalyst
    Maleki, Ali
    Ghassemi, Mina
    Eskandarpour, Vahid
    18TH INTERNATIONAL ELECTRONIC CONFERENCE ON SYNTHETIC ORGANIC CHEMISTRY, 2014,
  • [8] Using magnetic nanoparticles Fe3O4 as a reusable catalyst for the synthesis of pyran and pyridine derivatives via one-pot multicomponent reaction
    Heravi, Majid M.
    Beheshtiha, S. Yahya Shirazi
    Dehghani, Mahzad
    Hosseintash, Nastaran
    JOURNAL OF THE IRANIAN CHEMICAL SOCIETY, 2015, 12 (11) : 2075 - 2081
  • [9] Using magnetic nanoparticles Fe3O4 as a reusable catalyst for the synthesis of pyran and pyridine derivatives via one-pot multicomponent reaction
    Majid M. Heravi
    S. Yahya Shirazi Beheshtiha
    Mahzad Dehghani
    Nastaran Hosseintash
    Journal of the Iranian Chemical Society, 2015, 12 : 2075 - 2081
  • [10] Novel One-pot Synthesis of Pyrazolopyranopyrimidinones Using Newly Produced γ-Alumina Nanoparticles as Powerful Catalyst
    Sajad, Kiani
    Khodabakhshi, Saeed
    Alimorad, Rashidi
    Tavakoli, Ziba
    Dasthoon, Sadegh
    IRANIAN JOURNAL OF CHEMISTRY & CHEMICAL ENGINEERING-INTERNATIONAL ENGLISH EDITION, 2018, 37 (03): : 63 - 71