Influence of Heat Treatment Temperature on Microstructure and Bonding of TiO2 Film Coated on Diamond Particles Surface

被引:0
|
作者
刘小磐 [1 ,2 ]
KONG Weibing [1 ]
XIAO Haiyan [2 ]
TANG Hao [3 ]
WAN Long [1 ]
HU Weida [4 ]
王伟 [5 ,6 ,7 ]
机构
[1] School of Materials Science & Engineering, Hunan University
[2] State Key Laboratory of Silicate Materials for Architectures, Wuhan University of Technology
[3] Guangdong Feng Hua Advanced Technology (Holding) CO,LTD  4. School of Metallurgical Engineering, Hunan University of Technology  5. School of Au
[4] Hubei Province Key Laboratory of Modern Automotive Technology
[5] Hubei Province Automotive Parts Synergy Innovation Center
基金
中国国家自然科学基金;
关键词
diamond; TiO2; film; heat treatment temperature; chemical bond;
D O I
暂无
中图分类号
TB306 [];
学科分类号
0805 ; 080502 ;
摘要
TiO2films were coated on the surface of diamond particles using a sol-gel method. The effects of heat treatment temperature on the morphology, phase composition and chemical bond of diamond particles coated with TiO2films were investigated through SEM, TEM, X-ray diffraction analysis, Raman spectroscopy, FTIR, and XPS. The results showed that when being heat-treated at 600 ℃, the amorphous TiO2film transfered to the anatase film which bonded well with diamond substrate. Meanwhile, the Ti-O-C bond formed between TiO2film and diamond substrate. When being heat-treated at 800 ℃, TiO2film was still anatase, and partial diamond began to graphitize. The graphitizated carbon could also form the Ti-O-C bond with TiO2film, although TiO2film would tend to crack in this case.
引用
收藏
页码:1008 / 1012
页数:5
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