SYNTHESIS,CHARACTERIZATION AND CRYSTAL STRUCTURES OF η5-CH3C5H4)M（CO）2NO AND（η5-CH3C5H4）M（μ3-NH）(μ2-NO)（μ2-CO）Fe2（CO）6（M=Mo or W）

被引：0

作者：

Wen Hua SUN

Shi Yan YANG

Yuan Ci YIN Lanzhou Institute of Chemical Physics Chinese Academy of Sciences

Zhong Yuan ZHOU Chengdu Center of Analysis and Test Chinese Academy of Sciences

机构：

来源：

Chinese Chemical Letters | 1991年 / 03期

关键词：

Fe; M=Mo or W; CH3C5H4)M; AND; M; SYNTHESIS; CHARACTERIZATION AND CRYSTAL STRUCTURES OF; CO)Fe2; Mo; NO; NH;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

Synthesis of complexes（η;-CH;C;H;）M（CO）;NO（M=Mo,I;M=W,II）and clusters（η;-CH;C;H;）M（μ;-NH）(μ;-NO) （μ;-CO）Fe;（CO）;（M=Mo,III:M=W,IV）,based on the reaction of （η;-C5;）M（CO）;Cl with Na[Fe（CO）;NO] at room tem-perature,have been demonstrated,The crystal structures of II and IV arealso presented.

引用

页码：263 / 266

页数：4

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[1] NITROSYL COMPLEXES——SYNTHESIS, CHARACTERIZATION AND CRYSTAL STRUCTURES OF （η5-C5H5）M（CO）2NO AND （η5-C5H5）M（μ3-NH）(μ2-NO)（μ2-CO）Fe2（CO）6（M=Mo OR W）
杨世琰
孙文华
殷元骐
郁开北
周忠远
[J]. Science China Chemistry, 1991, (11) : 1304 - 1311
[2] Nitrosyl Complexes 6.Reactions of Na[Fe（CO）3NO]with Cp*M（CO）3Cl（Cp*=η5-CH3C5H4,M=Mo or W）:Crystal structures of Cp*M（CO）2NO and Cp*M（μ3-NH）(μ2-NO)（μ2-CO）Fe2（CO）6
SUN
[J]. Chinese Journal of Chemistry, 1993, (02) : 151 - 158
[3] NITROSYLCOMPLEXES——SYNTHESIS,CHARACTERIZATIONANDCRYSTALSTRUCTURESOF（η5-C5H5）M（CO）2NOAND（η5-C5H5）M（μ3-NH）(μ2-NO)（μ2-CO）Fe2（CO）6（M=MoORW）
杨世琰
孙文华
殷元骐
郁开北
周忠远
[J]. Science in China,Ser.B., 1991, Ser.B.1991 (11) - 1311
[4] Synthesis and photolysis of [M(CO)3H]2(η5,η5-C5H4CH2C5H4), where M = Mo and W.: Photochemical 'twist' rearrangement of M2(CO)6 (η5,η5-C5H4CH2C5H4) to give [M(CO)3][M(CO)3H](η5,η5:η1-C5H4CH2C5H3), where M = Mo and W.: The molecular structure [Mo(CO)3][Mo(CO)3Cl](η5,η5:η1-C5H4CH2C5H3)
Bitterwolf, TE
Saygh, A
Haener, JL
Fierro, R
Shade, JE
Rheingold, AL
Liable-Sands, L
Alt, HG
[J]. INORGANICA CHIMICA ACTA, 2002, 334 : 54 - 58
[5] 亚硝酰基配合物——Ⅱ.（η5-C5H5）M（CO）2NO和（η5-C5H5）M（μ3-NH）(μ2-NO)（μ2-CO）Fe2（CO）6（M=Mo或W）的合成、表征和晶体结构
杨世琰
孙文华
殷元骐
郁开北
周忠远
[J]. 中国科学:化学, 1991, (05) : 472 - 478
[6] NITROSYL COMPLEXES - SYNTHESIS, CHARACTERIZATION AND CRYSTAL-STRUCTURES OF (ETA-5-C5H5)M(CO)2NO AND (ETA-5-C5H5)-M(MU-3-NH)(MU-2-NO)(MU-2-CO)FE2(CO)6 (M = MO OR W)
YANG, SY
SUN, WH
YIN, YQ
YU, KB
ZHOU, ZY
[J]. SCIENCE IN CHINA SERIES B-CHEMISTRY, 1991, 34 (11): : 1304 - 1311
[7] Synthesis, Nujol matrix and solution photochemistry of M(CO)2[η5,η3-C5H4-C(CH3)2-C5H6] (where M = Cr or Mo):: molecular structures of Cr(CO)2[η5,η3-C5H4-C(CH3)2-C5H6], Mo(CO)2[η5,η3-C5H4-C(CH3)2-C5H6], and Mo(CO)[P(C6H5)3][η5,η3-C5H4-C(CH3)2-C5H6]
Bitterwolf, TE
Saygh, AA
Bays, JT
Weiss, CA
Scallorn, WB
Shade, JE
Rheingold, AL
Liable-Sands, L
[J]. JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1999, 583 (1-2) : 152 - 161
[8] Synthesis and photochemistry of ring-coupled heterobimetallic compounds of ruthenium.: The molecular structures of RuM(CO)5(μ-η5,η5-C5H4CR2C5H4), where M = Mo, R = CH3;: M = W, R = H, [Ru(CO)2][Mo(CO)3Cl](μ-η5,η1:η5-C5H4CH2C5H3) and [W(CO)3][Ru(CO)2Cl](μ-η5,η1:η5-C5H4CH2C5H3)
Bitterwolf, TE
Saygh, AA
Shade, JE
Rheingold, AL
Yap, GPA
Lable-Sands, LM
[J]. INORGANICA CHIMICA ACTA, 2000, 300 : 800 - 809
[9] Ring functionalized cyclopentadienyl derivatives of niobium and tantalum:: molecular structures of (η5-C5H4-CO2CH3)M(CO)4 where M = Nb and Ta and (η5-C5H4-CO2CH2C6H5)Nb(CO)4
Bitterwolf, TE
Gallagher, S
Rheingold, AL
Yap, GPA
[J]. JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1997, 545 : 27 - 33
[10] THE SYNTHESIS AND H-1-NMR STUDY OF VINYL ORGANOMETALLIC MONOMERS - (ETA-5-C5H4CH=CH2)M(CO)2(NO) (M=CR, MO, W) AND (ETA-5-C5H4CH=CH2)M(CO)2 (M=CO, RH, IR)
MACOMBER, DW
SPINK, WC
RAUSCH, MD
[J]. JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1983, 250 (01) : 311 - 318

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