Cleaner and convenient preparation of3-(4,6-dimethoxy-pyrimidin-2-yloxy)-2-methyl-phenol

被引：0
|
作者：
文岳中
方兆华
刘维屏
机构：
[1] China
[2] College of Environmental & Resource Sciences
[3] Hangzhou 310029
[4] Zhejiang University
[5] Institute of Environmental Science
来源：
Journal of Zhejiang University Science | 2004年 / 08期
关键词：
Cleaner preparation; Greener technology; Selective synthesis; 2-methyl-benzene-1; 3-diol; 3-(4; 6-dimeth- oxy-pyrimidin-2-yloxy)-2-methyl-phenol;
D O I：
暂无
中图分类号：
X383 [清洁工艺技术（无污染工艺）的研究];
学科分类号：
0822 ;
摘要：
Environmental concerns have highlighted the need of cleaner technologies. A cleaner, convenient and selective technology has been developed for the preparation of 3-(4,6-dimethoxy-pyrimidin-2-yloxy)-2-methyl-phenol (DPMP) from 2-methyl-benzene-1,3-diol in water as solvent. The isolated yield of DPMP is up to 86% in good selectivity. The product structure was characterized by conventional methods, H-NMR and MS. This technology belongs to the modern concept of 1 environmentally friendly low wastes or non-wastes technology (LWNWT).
引用
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页码：61 / 64
页数：4
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