Optimization of Reflux Extraction Process for Toosendanin from FRUCTUS TOOSENDAN

被引：0
|
作者：
LI Jie-yu1
2.Department of Pharmacy
3.Department of Pharmacy
机构：
来源：
Medicinal Plant | 2010年 / 12期
关键词：
FRUCTUS TOOSENDAN; Toosendanin; Reflux extraction; Optimization of extraction process; China;
D O I：
暂无
中图分类号：
TQ461 [中草药制剂的生产]; R284 [中药化学];
学科分类号：
1008 ;
摘要：
[Objective] Tto obtain the optimum reflux extraction conditions for toosendanin from FRUCTUS TOOSENDAN.[Method] Effects of extraction solvent,solid-liquid ratio,extraction temperature,extraction duration and extraction times on the yield of toosendanin were investigated using content of toosendanin as index which was determined by HPLC.[Result] The optimum reflux extraction conditions for toosendanin were proposed to be:extraction solvent of methanol,solid-liquid ratio of 1:30,extraction temperature of 80 ℃,extraction duration of 1.0 h,extraction times of 2.Under the optimum extraction process,the yield of toosendanin from FRUCTUS TOOSENDAN reached 1.344 9 mg/g.[Conclusion] Simple in process,reflux extraction method established in this study is effective and stable for extracting toosendanin from FRUCTUS TOOSENDAN.
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页码：66 / 69
页数：4
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