Zr/SBA-15复合材料的合成与表征

被引:0
|
作者
谢焕玲 [1 ]
徐文国 [1 ]
王丹 [2 ]
机构
[1] 北京理工大学理学院化学系
[2] 中国科学院过程工程研究所多相反应国家重点实验室
关键词
Zr/SBA-15复合材料; 前驱锆盐; 表征;
D O I
暂无
中图分类号
O643.36 [催化剂];
学科分类号
摘要
借助水热法,在酸性条件下直接加入合成系统前驱盐(硝酸锆或氧氯化锆),通过蒸发得到复合物,然后进行煅烧,制备Zr/SBA-15复合材料。利用X-射线粉末衍射和扫描电镜表征,结果显示此材料呈现二维六角密堆积结构,在Zr/Si摩尔比大于1/10时,合成材料中均出现锆的氧化物晶体相,且采用两种前驱盐合成材料形貌有很大的差别。
引用
收藏
页码:116 / 118+130 +130
页数:4
相关论文
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