Thermal Decomposition of Ammonium 3-Nitro-1,2,4-triazol-5-onate Monohydrate

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作者
LI Ji-zhen1
2. School of Science
3. School of Chemistry and Materials Science
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关键词
Ammonium 3-nitro-1,2,4-triazol-5-onate monohydrate; Thermal decomposition; DSC; TG; MS; IR;
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O626.2 [含双或多异原子的五节杂环];
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摘要
The thermal decomposition of ammonium 3-nitro-1,2,4-triazol-5-onate monohydrate[NH4(NTO)·H2O] was studied by means of thermal analysis-MS coupling and the combination technique of in situ thermolysis cell with rapid-scan Fourier transform infrared spectroscopy. The results show that there are two endothermic steps and one exothermic step in the decomposition process of NH4(NTO)·H2O. The detected gas products consist of NH3, H2O, N2, CO2, CO, and NO2.
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页码:786 / 789
页数:4
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