CdWO4纳米晶形貌可控合成

被引：1

作者：

杨琳琳 ^{[1
]}

王永刚 ^{[1
]}

魏超 ^{[1
]}

王玉江 ^{[1
]}

王晓峰 ^{[1
]}

徐刚 ^{[2
]}

韩高荣 ^{[2
]}

机构：

[1] 洛阳理工学院材料系

[2] 浙江大学材料系

来源：

人工晶体学报 | 2013年 / 42卷 / 07期

关键词：

形貌可控合成; 钨酸镉纳米晶; 水热法;

D O I：

10.16553/j.cnki.issn1000-985x.2013.07.035

中图分类号：

O611.4 [无机合成化学]; TB383.1 [];

学科分类号：

摘要：

分别以氯化镉、草酸镉、碳酸镉、柠檬酸镉和钨酸钠为原料,在没有采用模板和表面活性剂的条件下,采用水热法可控制备出了钨酸镉纳米颗粒、纳米棒、纳米束和纳米线。利用X射线衍射(XRD)、透射电镜(TEM)、高分辨透射电子显微镜(HRTEM)和选区电子衍射(SAED)对样品进行了表征。结果表明:[WO42-]/[Cd2+]摩尔比、反应时间及先驱体的类型对产物的形貌和尺寸有着重要的影响。

引用

页码：1414 / 1418

页数：5

共 10 条

[1] 脉冲电沉积结合水热法制备ZnS纳米条及其光学性质的研究
周英智
刘峥
袁帅
[J]. 人工晶体学报, 2012, 41 (05) : 1381 - 1385
[2] Besom-like CdWO4 structures composed of single-crystalline nanorods grown under a simple hydrothermal process in ultra-wide pH range
Hojamberdiev, Mirabbos
Kanakala, Raghunath
Ruzimuradov, Olim
Yan, Yinglin
Zhu, Gangqiang
Xu, Yunhua
[J]. OPTICAL MATERIALS, 2012, 34 (11) : 1954 - 1957
[3] Synthesis and characterization of CdWO4 nanocrystals
Priya, A. Mano
Selvan, R. Kalai
Senthilkumar, B.
Satheeshkumar, M. K.
Sanjeeviraja, C.
[J]. CERAMICS INTERNATIONAL, 2011, 37 (07) : 2485 - 2488
[4] Characterization and properties of Eu3+-doped CdWO4 prepared by a hydrothermal method
Dong Ye
Danzhen Li
Wei Chen
Yu Shao
Guangcan Xiao
Meng Sun
Xianzhi Fu
[J]. Research on Chemical Intermediates, 2009, 35 : 675 - 683
[5] Optical and luminescence properties of CdWO4 and CdWO4:Mo single crystals[J] . O. V. Rzhevskaya,D. A. Spasski?,V. N. Kolobanov,V. V. Mikha?lin,L. L. Nagornaya,I. A. Tupitsina,B. I. Zadneprovski?.Optics and Spectroscopy . 2008 (3)
[6] Morphology-controlled synthesis of CdWO 4 nanorods and nanoparticles via a molten salt method[J] . Yonggang Wang,Junfeng Ma,Jiantao Tao,Xiaoyi Zhu,Jun Zhou,Zhongqiang Zhao,Lijin Xie,Hua Tian.Materials Science ＆ Engineering B . 2006 (1)
[7] Polymer‐Assisted Hydrothermal Synthesis of Single‐Crystalline Tetragonal Perovskite PbZr[J] . G.Xu,Z.Ren,P.Du,W.Weng,G.Shen.Adv. Mater. . 2005 (7)
[8] Selective synthesis of CdWO4 short nanorods and nanofibers and their self-assembly
Wang, HL
Ma, XD
Qian, XF
Yin, J
Zhu, ZK
[J]. JOURNAL OF SOLID STATE CHEMISTRY, 2004, 177 (12) : 4588 - 4596
[9] Diode-pumped, self-stimulating, passively Q-switched Nd 3+ :PbWO 4 Raman laser[J] . Weibiao Chen,Yuji Inagawa,Takashige Omatsu,Mitsuhiro Tateda,Nobuo Takeuchi,Yoshiyuki Usuki.Optics Communications . 2001 (4)
[10] A New Photocatalyst CdWO4 Prepared with a Hydrothermal Method. Ye D,Li D,Zhang W,Sun M,Hu Y,Zhang Y,Fu X. J. Phys. Chem. C . 2008

← 1 →