Preparation of laurel oil alkanolamide from laurel oil

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[1] Kolancilar, Hakan
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Kolancilar, H. (alara_tr@yahoo.com) | 1600年 / American Oil Chemists' Society卷 / 81期
关键词：
Boiling liquids - Catalysis - Color - Esters - Ethanol - Evaporation - Fruits - Hydrochloric acid - Organic acids - Synthesis (chemical);
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摘要：
A low-temperature synthesis of laurel oil alkanolamides directly from laurel oil and ethanolamine was carried out in essentially quantitative yields. The ethanolamine/laurel oil molar ratio used was 10:1. Even though amine served as a catalyst in the reaction, we used sodium methoxide at a ratio of 0.2-2% as a second catalyst. The reaction was complete in 1-9 h at room temperature. The identity of the amide was confirmed by IR and 13C NMR spectroscopy.
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