α-Bi2O3 microcrystals and microrods: Thermal synthesis, structural and luminescence properties

被引：0
|
作者：
机构：
[1] Vila, M.
[2] Díaz-Guerra, C.
[3] Piqueras, J.
来源：
Díaz-Guerra, C. (cdiazgue@fis.ucm.es) | 1600年 / Elsevier Ltd卷 / 548期
关键词：
α-Bi2O3 microcrystals and microrods with pyramidal tips have been grown by a vapour-solid method using pure Bi as starting material. The morphology of the obtained microstructures depends on the annealing temperature and time. At 650 °C and for short annealing times; microcrystals with well defined facets and sizes of tens of microns; as well as clusters of microcrystals; are formed. Microrods were grown at 800 °C; mainly from nucleation sites in the clusters of microcrystals; and reach lengths of hundreds of microns. Micro-Raman spectroscopy measurements reveal the homogeneity of the obtained microstructures regarding the crystalline α-phase. The luminescence properties of the microrods have been investigated by cathodoluminescence in the scanning electron microscope and by photoluminescence in a confocal microscope. The obtained results were correlated with X-ray photoelectron spectroscopy measurements. © 2012 Elsevier B.V. All rights reserved;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
Journal article (JA)
引用
收藏
相关论文
共 50 条
  • [1] α-Bi2O3 microcrystals and microrods: Thermal synthesis, structural and luminescence properties
    Vila, M.
    Diaz-Guerra, C.
    Piqueras, J.
    JOURNAL OF ALLOYS AND COMPOUNDS, 2013, 548 : 188 - 193
  • [2] Synthesis and luminescence properties of hand-like α-Bi2O3 microcrystals
    Xiong, Ying
    Wu, Mingzai
    Ye, Jing
    Chen, Qianwang
    MATERIALS LETTERS, 2008, 62 (8-9) : 1165 - 1168
  • [3] Synthesis and field emission properties of hand-like Bi2O3 microcrystals
    Lin, J. Y.
    Zhang, Y. A.
    Wang, L. J.
    Yang, L.
    Guo, T. L.
    OPTOELECTRONIC MATERIALS, PTS 1AND 2, 2010, 663-665 : 50 - 53
  • [4] Synthesis and luminescence of single crystalline Bi2O3 nanosheets
    Fang GuoLi
    Chen Guang
    Wang Xiong
    Liu JinQiang
    SCIENCE CHINA-TECHNOLOGICAL SCIENCES, 2011, 54 (01) : 19 - 22
  • [5] Synthesis and luminescence of single crystalline Bi2O3 nanosheets
    GuoLi Fang
    Guang Chen
    Xiong Wang
    JinQiang Liu
    Science China Technological Sciences, 2011, 54 : 19 - 22
  • [6] Synthesis and luminescence of single crystalline Bi2O3 nanosheets
    FANG GuoLi
    Science China Technological Sciences, 2011, (01) : 19 - 22
  • [7] The Thermal Synthesis of the ZnO–Bi2O3 Pigments
    P. Šulcová
    M. Trojan
    Journal of Thermal Analysis and Calorimetry, 2000, 60 : 209 - 213
  • [8] Controllable synthesis of α-Bi2O3 and γ-Bi2O3 with high photocatalytic activity by α-Bi2O3→γ-Bi2O3→α-Bi2O3 transformation in a facile precipitation method
    Liu, Guo
    Li, Shuai
    Lu, Yuanyuan
    Zhang, Jing
    Feng, Zhaochi
    Li, Can
    JOURNAL OF ALLOYS AND COMPOUNDS, 2016, 689 : 787 - 799
  • [9] Structural and luminescence properties of Eu and Er implanted Bi2O3 nanowires for optoelectronic applications
    Vila, Maria
    Diaz-Guerra, Carlos
    Lorenz, Katharina
    Piqueras, Javier
    Alves, Eduardo
    Nappini, Silvia
    Magnano, Elena
    JOURNAL OF MATERIALS CHEMISTRY C, 2013, 1 (47) : 7920 - 7929
  • [10] Luminescence centers in α-Bi2O3 ceramics
    O. M. Bordun
    I. I. Kukharskii
    V. V. Dmitruk
    V. G. Antonyuk
    V. P. Savchin
    Journal of Applied Spectroscopy, 2008, 75 : 681 - 684
12345