Study on the Phase Equilibria of the Fe-Al-Ni-O System at 750°C

被引：0
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作者：
Du, Meng [1 ]
Mei, Haifeng [2 ,3 ]
Liu, Ya [2 ,3 ]
机构：
[1] College of Vehicle Engineering, Changzhou Vocational Institute of Mechatronic Technology, Changzhou,213164, China
[2] School of Materials Science and Engineering, Changzhou University, Changzhou,213164, China
[3] Jiangsu Key Laboratory of Materials Surface Science and Technology, Changzhou University, Changzhou,213164, China
来源：
Scanning | 2022年 / 2022卷
关键词：
X ray spectrometers - Scanning electron microscopy - Phase diagrams - Nickel oxide - Binary alloys - Film preparation - Corundum - Oxide films;
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摘要：
Phase equilibria of the Fe-Al-Ni-O system at 750°C were determined by scanning electron microscopy coupled with energy-dispersive X-ray spectrometer and X-ray power diffraction. 54 alloys were prepared with weighted metal and Ni2O3 powder and were annealed at 750°C for 45 days. Two four-phase equilibrium regions and three three-phase equilibrium regions were confirmed, and the boundary between spinel and corundum was obtained. Comparing with the Fe-Al-Ni-O oxidation diagram at 750°C calculated with FSstel and FToxid databases, the phase boundary of the spinel and corundum oxides from experiments was inclined to the Ni-Al side. The determined relationship between primary oxides and alloy composition in this work can be used as a reference for the preparation of the oxide film by selective oxidation. Copyright © 2022 Meng Du et al.
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