Isolation and purification of alkaloids from plumula nelumbinis by double-column adsorption chromatography

被引：0
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作者：
Zhang, Jixiang [1 ]
Guo, Jinsheng [1 ]
Yang, Jialing [3 ]
Ou, Lailiang [2 ]
机构：
[1] Department of Chemistry, Langfang Normal College, Langfang 065000, China
[2] Key Laboratory of Bioactive Materials, Ministry of Education, Institute of Molecular Biology, Nankai University, Tianjin 300071, China
[3] Tianjin Product Quality Inspection Technology Research Institute, Tianjin 300384, China
来源：
Lizi Jiaohuan Yu Xifu/Ion Exchange and Adsorption | 2008年 / 24卷 / 06期
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摘要：
The performance of adsorption and separation for liensinine, isoliensinine and neferine was studied by double-column adsorption chromatography using macroporous adsorption and cation exchange resins. The alkaloid extract with 49.2% total contents by mass representing 10.6% liensinine, 10.6% isoliensinine and 28.0% neferine respectively was prepared by D72 cation exchange resins, in which most of the impurities were water-soluble alkaloids. Furthermore, the alkaloid extract with 82.6% total contents by mass containing 33.1%, 15.0% and 34.5% of the three adsorbates respectively was prepared by double-column adsorption chromatography using AKS-W macroporous adsorption and D72 cation exchange resins. As a result, the content of single and total alkaloids has been greatly increased by the double-column adsorption chromatography.
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页码：512 / 517
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