Hydrothermal synthesis and crystal structure of a novel layered compound [Ni(C10H8N2)2V3O 8.5]

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Luan, G.-Y.
Wang, E.-B.
Han, Z.-B.
Li, Y.-G.
Lu, Y.
Hu, C.-W.
Hu, N.-H.
Jia, H.-Q.
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A novel layered compound, [Ni(C10H8N2)2V3O 8.5], was hydrothermally synthesized and structurally characterized by single crystal X-ray diffraction. The compound crystallizes in monoclinic system, space group P21/c with a=1.551 8(3) nm, b=1.476 1(3) nm, c=1.048 3(2) nm, β=92. 02(3)°, V = 2.399 8(8) nm3 Z=4, R=0.046 7, wR2=0.085 9.
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页码:1290 / 1291
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