Solid-state compounds of 4-chlorobenzylidenepyruvate with lanthanides preparation and thermal studies

被引:0
|
作者
Fernandes, N.S. [1 ]
Carvalho Filho, M.A.S. [1 ]
Melios, C.B. [1 ]
Ionashiro, M. [1 ]
机构
[1] Inst. de Quim. de Araraquara, UNESP, C P. 355, SP. CEP, 14801-970, Brazil
关键词
Differential scanning calorimetry - Lanthanum compounds - Pyrolysis - Stoichiometry - Thermal effects - Thermodynamic stability - Thermogravimetric analysis - X ray powder diffraction;
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摘要
Solid-state compounds Ln-4Cl-BP, where Ln represents lighter trivalent lanthanides and 4Cl-BP is 4-chlorobenzylidenepyruvate, were prepared. Thermogravimetry, derivative thermogravimetry (TG and DTG), differential scanning calorimetry (DSC) and other methods of analysis were used to characterize and to study the thermal behaviour of these compounds.
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页码:663 / 668
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