Synthesis and characterization of in situ polymerized poly(methyl methacrylate)-cerium molybdate nanocomposite for electroanalytical application

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作者：
Khan, Asif Ali [1 ]
Paquiza, Leena [1 ]
机构：
[1] Khan, Asif Ali
[2] Paquiza, Leena
来源：
Khan, A.A. (asifkhan42003@yahoo.com) | 1600年 / John Wiley and Sons Inc卷 / 127期
关键词：
In the present study; a new technique to synthesize composites of poly(methyl methacrylate) cerium molybdate (PMMA-CeMoO4) is reported. The study concerns the characterization of poly(methyl methacrylate; PMMA) and PMMA-CeMoO4 nanocomposites are also discussed. The physical properties of the material were described using TGA-DTA; FTIR; X-ray; TEM; and SEM studies. The adsorption efficiency towards heavy metal ions was determined by distribution studies and material was found to be highly selective for lead; a heavy toxic metal ion; indicating the utility of the synthesized material for the removal of this ion from the waste stream. The material was used as electroactive component for the construction of an ion-selective membrane electrode. The membrane electrode was mechanically stable; having wide dynamic range; with quick response time and could be operated for at least 5 months without any considerable divergence in the potential response characteristics. The electrode was successfully used as indicator electrode in complexation titrations. Copyright © 2012 Wiley Periodicals; Inc;
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页码：3737 / 3748
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