Preparation of Zirconium Praseodymium Yellow Pigments for Ceramic Inkjet Printing by Sol-gel Method

被引：0
|
作者：
Xu X. [1 ]
Guan X. [1 ]
Wu J. [1 ]
Zhang C. [1 ]
Sang Y. [1 ]
Liu X. [1 ]
机构：
[1] State Key Laboratory of Silicate Materials for Architectures, Wuhan University of Technology, Wuhan
来源：
| 2017年 / Chinese Ceramic Society卷 / 45期
关键词：
Ceramic ink-jet printing; Sol-gel method; Zirconium praeodymium yellow pigments;
D O I：
10.14062/j.issn.0454-5648.2017.06.16
中图分类号：
学科分类号：
摘要：
Pr-Zircon yellow pigment with small particle size and good homogeneity was prepared by a sol-gel method. Based on the colorimetric evaluation according to the CIE L*a*b* color system, the sample was obtained under optimum condition (i.e., adopted Pr of 3%, solution pH value of 3 and a bath-temperature of 70℃). The colorimetric parameters of optimal sample are the lightness of 90.37, yellow-blue value of 40.50, red-green value close to 0 (-0.33), indicating a pure yellow color with less interference of red-green color. The results by X-ray diffraction show that the sample contains zirconium silicate as a major phase with a small amount of β-quartz and monoclinic zirconia. The analysis by transmission electron microscopy reveals that Zr ions in zirconium silicate are partially substituted by Pr ions, the grain size of well-grown crystal is 62 nm, and a tetragonal structure with clear crystal stripes appears. According to the analysis of decoration effect of prepared inks, Pr-Zircon yellow pigment has a pure yellow color glaze effect. © 2017, Editorial Department of Journal of the Chinese Ceramic Society. All right reserved.
引用
收藏
页码：855 / 862
页数：7
相关论文
共 14 条
  • [1] Zhu B., Preparation of praseodymium doped zircon yellow ceramic pigment for ceramic ink and research on the color mechanism, (2016)
  • [2] Magdassi S., Eron G., Vinetsky Y., Et al., Ink for ceramic surfaces
  • [3] Kar J.K., Stevens R., Bowen C.R., Processing and characterization of Pr-zircon pigment powder, Adv Appl Ceram, 104, 5, pp. 233-238, (2005)
  • [4] Lin W., Li X., Xu P., Et al., J Qiqihar Univ, 31, 2, pp. 12-14, (2015)
  • [5] Liu R., Development of praseodymium doped zircon pigments for ceramic ink-jet printing inks, (2015)
  • [6] Cao K., Guo X., Gao Y., Et al., J Inorg Mater, 27, 9, pp. 984-990, (2012)
  • [7] Li G., Zheng M., Wang X., Et al., J Ceram, 21, 9, pp. 162-165, (2000)
  • [8] Jin B., Research on the synthesis of the zircon pigments and the ceramic ink, (2014)
  • [9] Nero G.D., Cappelletti G., Ardizzone S., Et al., Yellow Pr-zircon pigments, J Eur Ceram Soc, 24, 17, pp. 3603-3611, (2004)
  • [10] Zhai X., Chin Ceram, 6, pp. 32-33, (2007)
12