Synthesis, structure and Hirshfeld surface analysis of pyridinium derivative crystals

被引：0
|
作者：
Balasubramanian, V. [1 ]
Guganathan, L. [2 ]
Arockiam, S. Ignatius [3 ]
Balakrishnan, C. [4 ]
机构：
[1] Sona Coll Technol, Dept Phys, Salem, India
[2] Saveetha Insitute Med & Tech Sci, Saveetha Sch Engn, Dept Phys, Chennai, India
[3] GTN Arts Coll, Dept Chem, Dindigul, India
[4] Erode Sengunthar Engn Coll, Dept Chem, Erode 638057, Tamil Nadu, India
来源：
MOLECULAR CRYSTALS AND LIQUID CRYSTALS | 2024年
关键词：
Fingerprint plot; pyridinium crystal; supramolecular assembly; thermal stability; GROWTH; PICRATE;
D O I：
10.1080/15421406.2024.2390295
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Slow evaporation methods were employed to grow single crystals of 3-acetylpyridinium picrate (I), 4-acetylpyridinium picrate (II), and pyridin-4-ylmethanaminium 2,2-diphenylacetate hydrate (III). Crystal (I) and (III) crystallize triclinic crystal system with a centric (P & imacr;) space group and (II) crystallize in a monoclinic system with a centric (P21/c) space group. Various types of non-covalent interactions take part successfully in the construction of 3D networks in the compounds. Optical reflectance measurements showed 2.57, 2.66, and 4.45 eV as band gaps for (I), (II) and (III) respectively. TG/DTA analysis reveals the thermal pattern of the compounds. Intermolecular interactions are quantified by Hirshfeld surface analysis.
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页数：13
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