Extraction of microcrystalline cellulose from Ficus benghalensis leaf and its characterization

被引:10
|
作者
Narayanaperumal, Sunesh [1 ]
Divakaran, Divya [2 ]
Suyambulingam, Indran [3 ,4 ]
Singh, Manoj Kumar [2 ]
Sanjay, M. R. [2 ]
Siengchin, Suchart [2 ]
机构
[1] Rohini Coll Engn & Technol, Dept Mech Engn, Kanyakumari 629401, Tamil Nadu, India
[2] King Mongkuts Univ Technol North Bangkok KMUTNB, Sirindhorn Int Thai German Sch Engn TGGS, Dept Mat & Prod Engn, Nat Composites Res Grp Lab, Bangkok 10800, Thailand
[3] Alliance Univ, Alliance Coll Engn & Design, Dept Mech Engn, Bengaluru 562106, Karnataka, India
[4] Alliance Univ, Alliance Coll Engn & Design, Ctr Res, Bengaluru 562106, Karnataka, India
关键词
Ficus Benghalensis; Cellulose; Carbohydrates; Bio filler; Biopolymer; AGRO-WASTE; STRAW; MCC;
D O I
10.1016/j.ijbiomac.2024.134394
中图分类号
Q5 [生物化学]; Q7 [分子生物学];
学科分类号
071010 ; 081704 ;
摘要
Microcrystalline cellulose (MCC) is a crucial component in various industries, including pharmaceuticals, culinary, and cosmetics. The growing demand for MCC has spurred research into extraction methods. This study focused on extracting MCC from Ficus benghalensis using acid hydrolysis to convert the alpha-cellulose content of its leaves into MCC. The solvent used in this process was recyclable for further use. The extracted MCC was characterized by its physicochemical properties, including density, yield percentage, and structural characteristics. The yield was approximately 39.68 %, and the density was low at 1.518 g/cm3, making it suitable for filler applications. Fourier transform spectroscopy and UV-visible analysis identified functional groups of cellulose. Xray diffraction analysis revealed a crystallite size of 1.560 nm and a crystallinity index of 66.43 %, indicating suitability for related applications. ImageJ determined a mean particle size of 36.545 mu m, while scanning electron microscopy showed distinct surface orientations. Atomic force microscopy revealed surface roughness, root mean square, ten-point average roughness, skewness, and kurtosis. Elemental analysis indicated high concentrations of carbon (20.1 %) and oxygen (34 %). Based on these physicochemical features, the extracted MCC could be a valuable source for applications such as filler in reinforcement technology and coating material in pharmaceutical products.
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页数:13
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